10-Nitroacenaphtho[1,2-b]quinoline

Base Information

Chemical Name:10-Nitroacenaphtho[1,2-b]quinoline
CAS No.:94223-88-8
Molecular Formula:C₁₉H₁₀N₂O₂
Molecular Weight:298.301
Hs Code.:2933990090
Mol file:94223-88-8.mol

Synonyms:10-Nitro-acenaphtho(1,2-b)quinoline;10-Nitroacenaphtho(1,2-b)quinoline;10-Nitroacenaphtho[1,2-b]quinoline;94223-88-8;Acenaphtho[1,2-b]quinoline, 10-nitro-;CCRIS 6582

Suppliers and Price of 10-Nitroacenaphtho[1,2-b]quinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 10-Nitroacenaphtho[1,2-b]quinoline

Chemical Property:

Vapor Pressure:3.4E-09mmHg at 25°C
Boiling Point:487.9°Cat760mmHg
Flash Point:218.9°C
PSA：12.89000
Density:1.3g/cm³
LogP:5.34380
XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:298.074227566
Heavy Atom Count:23
Complexity:490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C3C(=C1)C4=C(C3=CC=C2)N=C5C=CC(=CC5=C4)[N+](=O)[O-]

Technology Process of 10-Nitroacenaphtho[1,2-b]quinoline

There total 3 articles about 10-Nitroacenaphtho[1,2-b]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 94223-83-3
(4-Nitro-phenyl)-(2-{[(E)-4-nitro-phenylimino]-methyl}-acenaphthylen-1-yl)-amine; hydrochloride

: 94223-88-8
10-Nitro-acenaphtho[1,2-b]quinoline

Guidance literature:: Heating;
DOI:10.1016/S0040-4020(01)91307-9

Reference yield:

: 13152-84-6
2-chloroacenaphthylene-1-carbaldehyde

: 94223-88-8
10-Nitro-acenaphtho[1,2-b]quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 2 N HCl / ethanol / 1.) room temp., 2 h, 2.) reflux 15 min

2: 80 percent / Heating

With hydrogenchloride; In ethanol;
DOI:10.1016/S0040-4020(01)91307-9

Reference yield:

: 2235-15-6
1(2H)-acenaphthylenone

: 94223-88-8
10-Nitro-acenaphtho[1,2-b]quinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / POCl₃ / 1.) from 0 deg C to room temp., 1 h, 2.) 60-70 deg C, 6 h

2: 91 percent / 2 N HCl / ethanol / 1.) room temp., 2 h, 2.) reflux 15 min

3: 80 percent / Heating

With hydrogenchloride; trichlorophosphate; In ethanol;
DOI:10.1016/S0040-4020(01)91307-9