2-Benzoyl-6,7,8,9-tetrahydro-5-methoxyimidazo[1,2-a]quinazoline

Base Information

• Chemical Name: 2-Benzoyl-6,7,8,9-tetrahydro-5-methoxyimidazo[1,2-a]quinazoline
• CAS No.: 90807-98-0
• Molecular Formula: C18H17N3O2
• Molecular Weight: 307.35
• Mol file: 90807-98-0.mol

Synonyms:(5-Methoxy-6,7,8,9-tetrahydro-imidazo[1,2-a]quinazolin-2-yl)-phenyl-methanone;

Chemical Property of 2-Benzoyl-6,7,8,9-tetrahydro-5-methoxyimidazo[1,2-a]quinazoline

Chemical Property:

• Melting Point: 234 °C
• PSA: 56.49000
• LogP: 2.84770

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-Benzoyl-6,7,8,9-tetrahydro-5-methoxyimidazo[1,2-a]quinazoline

There total 2 articles about 2-Benzoyl-6,7,8,9-tetrahydro-5-methoxyimidazo[1,2-a]quinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-1-phenylpropane-1,2-dione (29634-62-6) + 4-Methoxy-5,6,7,8-tetrahydro-quinazolin-2-ylamine (90808-73-4) → (5-methoxy-6,7,8,9-tetrahydroimidazol[1,2-a]quinazolin-2-yl)-phenylmethanone (90807-98-0)

Guidance literature:

Yield given. Multistep reaction; 1.) THF, 4 h, 2.) EtOH, reflux, 3 h;

DOI:10.1021/jm00401a025

Reference yield:

→ (5-methoxy-6,7,8,9-tetrahydroimidazol[1,2-a]quinazolin-2-yl)-phenylmethanone (90807-98-0)

Guidance literature:

Reference yield: 80.0%

(5-methoxy-6,7,8,9-tetrahydroimidazol[1,2-a]quinazolin-2-yl)-phenylmethanone (90807-98-0) → (1-bromo-5-methoxy-6,7,8,9-tetrahydroimidazo<1,2-a>quinazolin-2-yl)phenylmethanone (114095-17-9)

Guidance literature:

With N-Bromosuccinimide; In chloroform; for 0.166667h;

DOI:10.1021/jm00401a025

upstream raw materials:

3-bromo-1-phenylpropane-1,2-dione

4-Methoxy-5,6,7,8-tetrahydro-quinazolin-2-ylamine

Downstream raw materials:

(1-bromo-5-methoxy-6,7,8,9-tetrahydroimidazo<1,2-a>quinazolin-2-yl)phenylmethanone

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