Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate

Base Information

Chemical Name:Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate
CAS No.:83763-15-9
Molecular Formula:C₁₅H₁₇N₃O₃
Molecular Weight:287.318
Hs Code.:
European Community (EC) Number:280-699-9
UNII:87F98555KA
DSSTox Substance ID:DTXSID00232607
Nikkaji Number:J296.185G
Wikidata:Q27269824
Mol file:83763-15-9.mol

Synonyms:83763-15-9;Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate;UNII-87F98555KA;EINECS 280-699-9;87F98555KA;Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-2H-pyridine-1-carboxylate;DTXSID00232607;Q27269824;1(2H)-PYRIDINECARBOXYLIC ACID, 4-(2,3-DIHYDRO-2-OXO-1H-BENZIMIDAZOL-1-YL)-3,6-DIHYDRO-, ETHYL ESTER;4-[(2,3-Dihydro-2-oxo-1H-benzimidazol)-1-yl]-3,6-dihydro-1(2H)-pyridinecarboxylic acid ethyl ester;ETHYL-3,6-DIHYDRO-4-(2,3-DIHYDRO-2-OXO-1H-BENZIMIDAZOLE-1-YL)-1(2H)PYRIDINECARBOXYLATE

Suppliers and Price of Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate

Chemical Property:

PSA：67.59000
Density:1.313g/cm³
LogP:2.38290
XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:287.12699141
Heavy Atom Count:21
Complexity:463

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)N1CCC(=CC1)N2C3=CC=CC=C3NC2=O

Technology Process of Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate

There total 2 articles about Ethyl 4-(2,3-dihydro-2-oxo-1H-benzimidazol-1-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 959700-75-5
1,3-dihydrospiro[2H-benzimidazole-2,4'-piperidine]-1'-carboxylic acid ethyl ester

: 32315-10-9
bis(trichloromethyl) carbonate

: 83763-15-9
4-(2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)-3,6-dihydro-2H-pyridine-1-carboxylic acid ethyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.tet.2007.06.106

Reference yield: 4.0%

: 959700-75-5
1,3-dihydrospiro[2H-benzimidazole-2,4'-piperidine]-1'-carboxylic acid ethyl ester

: 32315-10-9
bis(trichloromethyl) carbonate

: 53786-47-3
4-(2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)-piperidine-1-carboxylic acid ethyl ester

: 83763-15-9
4-(2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)-3,6-dihydro-2H-pyridine-1-carboxylic acid ethyl ester

Guidance literature:: With sodium tris(acetoxy)borohydride; In tetrahydrofuran; for 0.25h; Title compound not separated from byproducts.;
DOI:10.1016/j.tet.2007.06.106