(1S,2R)-(-)-2-AMINOCYCLOHEX-3-ENECARBOXYLIC ACID HYDROCHLORIDE

Base Information

• Chemical Name: (1S,2R)-(-)-2-AMINOCYCLOHEX-3-ENECARBOXYLIC ACID HYDROCHLORIDE
• CAS No.: 132487-40-2
• Molecular Formula: C₇H₁₁NO₂*ClH
• Molecular Weight: 177.631
• Hs Code.: 2922498590
• Mol file: 132487-40-2.mol

Synonyms:3-Cyclohexene-1-carboxylicacid, 2-amino-, hydrochloride, (1S,2R)- (9CI); 3-Cyclohexene-1-carboxylic acid,2-amino-, hydrochloride, (1S-cis)-

Chemical Property of (1S,2R)-(-)-2-AMINOCYCLOHEX-3-ENECARBOXYLIC ACID HYDROCHLORIDE

Chemical Property:

• Melting Point: 192-209 °C
• Boiling Point: 285°Cat760mmHg
• Flash Point: 126.2°C
• PSA: 63.32000
• Density: 1.18g/cm³
• LogP: 1.86680

Purity/Quality:

98%min ^*data from raw suppliers

(1S,2R)-2-Aminocyclohex-3-enecarboxylic acid hydrochloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 34
• Safety Statements: 45-36/37/39-26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1S,2R)-(-)-2-AMINOCYCLOHEX-3-ENECARBOXYLIC ACID HYDROCHLORIDE

There total 6 articles about (1S,2R)-(-)-2-AMINOCYCLOHEX-3-ENECARBOXYLIC ACID HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(1S,6R)-7-azabicyclo[4.2.0]oct-4-en-8-one (285560-99-8) → (1S,2R)-2-aminocyclohex-3-enecarboxylic acid hydrochloride (131783-54-5,132487-40-2,142035-00-5)

Guidance literature:

With hydrogenchloride; In water; for 3h; Heating;

DOI:10.1016/j.tetasy.2004.05.029

Reference yield: 76.0%

(1S,6R)-7-azabicyclo[4.2.0]octan-8-one → (1S,2R)-2-aminocyclohex-3-enecarboxylic acid hydrochloride (131783-54-5,132487-40-2,142035-00-5)

Guidance literature:

With hydrogenchloride; water; at 0 ℃; for 1h;

DOI:10.3390/molecules201219749

Reference yield:

ethyl cis-(2-aminocyclohex-3-ene)-1-carboxylate → C7H11NO2*HCl (131783-54-5,132487-40-2,142035-00-5)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O / Candida antarctica lipase B / diisopropyl ether / 66 h / 65 °C

2: 472 mg / aq. HCl / 4 h / Heating

With hydrogenchloride; water; Candida antarctica lipase B; In di-isopropyl ether;

DOI:10.1002/chem.200700257

upstream raw materials:

(1S,6R)-7-azabicyclo[4.2.0]oct-4-en-8-one

cis-2-aza-3-oxobicyclo<4.2.0>octane

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