2-(4-Chlorophenylthio)cyclohexanone

Base Information

Chemical Name:2-(4-Chlorophenylthio)cyclohexanone
CAS No.:5409-84-7
Molecular Formula:C12H13ClOS
Molecular Weight:240.754
Hs Code.:
NSC Number:12536
DSSTox Substance ID:DTXSID301287010
Nikkaji Number:J2.579.734E

Synonyms:5409-84-7;2-[(4-CHLOROPHENYL)SULFANYL]CYCLOHEXAN-1-ONE;NSC12536;2-(4-Chlorophenylthio)cyclohexanone;DTXSID301287010;NSC-12536;AKOS005216912;AKOS017010584;2-[(4-Chlorophenyl)thio]cyclohexanone;EN300-394805

Suppliers and Price of 2-(4-Chlorophenylthio)cyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-(4-Chlorophenylthio)cyclohexanone

Chemical Property:

Vapor Pressure:7.85E-06mmHg at 25°C
Boiling Point:375.3°Cat760mmHg
Flash Point:180.8°C
Density:1.24g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:240.0375639
Heavy Atom Count:15
Complexity:224

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=O)C(C1)SC2=CC=C(C=C2)Cl

Technology Process of 2-(4-Chlorophenylthio)cyclohexanone

There total 5 articles about 2-(4-Chlorophenylthio)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 106-54-7
p-Chlorothiophenol

: 5409-84-7
2-(4-chloro-phenylsulfanyl)-cyclohexanone

Guidance literature:: With N-chloro-succinimide; In dichloromethane; at 20 ℃; for 0.7h;
DOI:10.1016/j.tetlet.2008.02.136

Reference yield: 63.0%

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 5409-84-7
2-(4-chloro-phenylsulfanyl)-cyclohexanone

Guidance literature:: With potassium phosphate; In dimethyl sulfoxide; at 40 ℃; for 18h;
DOI:10.1007/s00706-014-1188-7

Reference yield: 38.0%

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 110452-14-7
2-phenylthiocyclohexanone

: 5409-84-7
2-(4-chloro-phenylsulfanyl)-cyclohexanone

Guidance literature:: With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; Inert atmosphere; Reflux;
DOI:10.1248/cpb.58.1349