Lyciumin A

Base Information

Chemical Name:Lyciumin A
CAS No.:125708-06-7
Molecular Formula:C42H51 N9 O12
Molecular Weight:873.92
Hs Code.:
Wikidata:Q104402518
Mol file:125708-06-7.mol

Synonyms:Lyciumin A;125708-06-7;11-(hydroxymethyl)-2-[[3-(4-hydroxyphenyl)-2-[[1-(5-oxopyrrolidine-2-carbonyl)pyrrolidine-2-carbonyl]amino]propanoyl]amino]-3,6,9,12-tetraoxo-5-propan-2-yl-1,4,7,10,13-pentazatricyclo[14.6.1.017,22]tricosa-16(23),17,19,21-tetraene-14-carboxylic acid;LyciuminA;CHEBI:172844;AKOS040756589

Suppliers and Price of Lyciumin A

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Lyciumin A

Chemical Property:

XLogP3:0.3
Hydrogen Bond Donor Count:10
Hydrogen Bond Acceptor Count:12
Rotatable Bond Count:10
Exact Mass:873.36571810
Heavy Atom Count:63
Complexity:1760

Purity/Quality:: ≥98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C1C(=O)NCC(=O)NC(C(=O)NC(CC2=CN(C(C(=O)N1)NC(=O)C(CC3=CC=C(C=C3)O)NC(=O)C4CCCN4C(=O)C5CCC(=O)N5)C6=CC=CC=C26)C(=O)O)CO

Technology Process of Lyciumin A

There total 6 articles about Lyciumin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 145396-92-5
C₄₃H₅₃N₉O₁₂

: 125708-06-7
lyciumin A

Guidance literature:: With lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1039/c39920001353

Reference yield:

: 145396-91-4
(5S,11S,14S)-2-Benzyloxycarbonylamino-11-hydroxymethyl-5-isopropyl-3,6,9,12-tetraoxo-1,4,7,10,13-pentaaza-tricyclo[14.6.1.0^17,22]tricosa-16⁽²³⁾,17⁽²²⁾,18,20-tetraene-14-carboxylic acid methyl ester

: 125708-06-7
lyciumin A

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / Pd/C / dimethylformamide / 2 h

2: 64 percent / 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium tetrafluoroborate (TBTU) / dimethylformamide

3: 100 percent / aq. LiOH / dimethylformamide / 2 h / 20 °C

With lithium hydroxide; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1039/c39920001353

Reference yield:

: (S)-2-((S)-2-Amino-3-hydroxy-propionylamino)-3-(1-{benzyloxycarbonylamino-[(S)-2-methyl-1-(pentafluorophenyloxycarbonylmethyl-carbamoyl)-propylcarbamoyl]-methyl}-1H-indol-3-yl)-propionic acid methyl ester

: 125708-06-7
lyciumin A

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaHCO₃ / CH₂Cl₂

2: 100 percent / H₂ / Pd/C / dimethylformamide / 2 h

3: 64 percent / 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium tetrafluoroborate (TBTU) / dimethylformamide

4: 100 percent / aq. LiOH / dimethylformamide / 2 h / 20 °C

With lithium hydroxide; hydrogen; sodium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39920001353