3-Chloro-4'-methylbenzophenone

Base Information

Chemical Name:3-Chloro-4'-methylbenzophenone
CAS No.:13395-60-3
Molecular Formula:C14H11 Cl O
Molecular Weight:230.694
Hs Code.:2914700090
DSSTox Substance ID:DTXSID40158433
Nikkaji Number:J2.296.750I
Wikidata:Q83026697
Mol file:13395-60-3.mol

Synonyms:3-Chloro-4'-methylbenzophenone;13395-60-3;(3-chlorophenyl)-(4-methylphenyl)methanone;BRN 2259802;BENZOPHENONE, 3-CHLORO-4'-METHYL-;3-chloro-4/'-methylbenzophenone;(3-chlorophenyl)(4-methylphenyl)methanone;3-07-00-02130 (Beilstein Handbook Reference);SCHEMBL2924646;DTXSID40158433;MVYBBEGJXRCIGB-UHFFFAOYSA-N;(3-Chloro-phenyl)-p-tolyl-methanone;MFCD01662298;Benzophenone, 3-chloro-4/'-methyl-;AKOS009347195;LS-38884;AE-641/00008040;J-006460

Suppliers and Price of 3-Chloro-4'-methylbenzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
3-Chloro-4'-methylbenzophenone 97%
2g
$ 539.00

Rieke Metals
3-Chloro-4'-methylbenzophenone 97%
1g
$ 294.00

Rieke Metals
3-Chloro-4'-methylbenzophenone 97%
5g
$ 968.00

Matrix Scientific
3-Chloro-4'-methylbenzophenone
5g
$ 930.00

Matrix Scientific
3-Chloro-4'-methylbenzophenone
2g
$ 551.00

Matrix Scientific
3-Chloro-4'-methylbenzophenone
1g
$ 319.00

Crysdot
3-Chloro-4'-methylbenzophenone 95+%
1g
$ 316.00

Crysdot
3-Chloro-4'-methylbenzophenone 95+%
5g
$ 922.00

American Custom Chemicals Corporation
3-CHLORO-4'-METHYLBENZOPHENONE 95.00%
1G
$ 1019.93

Total 10 raw suppliers

Chemical Property of 3-Chloro-4'-methylbenzophenone

Chemical Property:

Boiling Point:368.5°Cat760mmHg
Flash Point:198.8°C
PSA：17.07000
Density:1.178g/cm³
LogP:3.87940
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:230.0498427
Heavy Atom Count:16
Complexity:243

Purity/Quality:

98%Min ^*data from raw suppliers

3-Chloro-4'-methylbenzophenone 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C2=CC(=CC=C2)Cl

Technology Process of 3-Chloro-4'-methylbenzophenone

There total 8 articles about 3-Chloro-4'-methylbenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 106-38-7
para-bromotoluene

: 587-04-2
m-Chlorobenzaldehyde

: 13395-60-3
(3-chlorophenyl)(4-methylphenyl)methanone

Guidance literature:: para-bromotoluene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

m-Chlorobenzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h;

With iodine; potassium carbonate; In tert-butyl alcohol; for 3h; Reflux;
DOI:10.1016/j.tet.2011.12.023

Reference yield: 82.0%

: 5720-05-8
4-methylphenylboronic acid

: 587-04-2
m-Chlorobenzaldehyde

: 13395-60-3
(3-chlorophenyl)(4-methylphenyl)methanone

Guidance literature:: With potassium phosphate; water; C₃₄H₂₉BN₂O₂OsP₂; In toluene; at 100 ℃; for 24h;
DOI:10.1021/acs.organomet.1c00533

Reference yield: 51.0%

: 106-38-7
para-bromotoluene

: 63503-60-6
3-chlorophenylboronic acid

: benzene-1,3,5-triyl triformate

: 13395-60-3
(3-chlorophenyl)(4-methylphenyl)methanone

Guidance literature:: With 5% Pd/C; triethylamine; In tetrahydrofuran; at 100 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1002/asia.202100540