Ethyl 4-(4-chlorophenyl)-2-(furan-2-carbonylamino)thiophene-3-carboxylate

Base Information

• Chemical Name: Ethyl 4-(4-chlorophenyl)-2-(furan-2-carbonylamino)thiophene-3-carboxylate
• CAS No.: 6240-36-4
• Molecular Formula: C₁₆H₂₄O₂
• Molecular Weight: 248.365
• DSSTox Substance ID: DTXSID40359665
• Wikidata: Q82140964

Synonyms:6240-36-4;ethyl 4-(4-chlorophenyl)-2-(furan-2-carbonylamino)thiophene-3-carboxylate;Ethyl 4-(4-chlorophenyl)-2-(furan-2-carboxamido)thiophene-3-carboxylate;CBMicro_003364;DTXSID40359665;SMSF0018870;ethyl 4-(4-chlorophenyl)-2-(furan-2-amido)thiophene-3-carboxylate;STK876725;AKOS001036969;CB05104;BIM-0003317.P001;SR-01000477428;SR-01000477428-1;Z30498505;ethyl 4-(4-chlorophenyl)-2-(2-furoylamino)-3-thiophenecarboxylate;ethyl 4-(4-chlorophenyl)-2-[(furan-2-ylcarbonyl)amino]thiophene-3-carboxylate

Chemical Property of Ethyl 4-(4-chlorophenyl)-2-(furan-2-carbonylamino)thiophene-3-carboxylate

Chemical Property:

• Vapor Pressure: 5.05E-08mmHg at 25°C
• Boiling Point: 442.4°Cat760mmHg
• Flash Point: 221.3°C
• Density: 1.38g/cm³
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 6
• Exact Mass: 375.0332068
• Heavy Atom Count: 25
• Complexity: 484

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)C1=C(SC=C1C2=CC=C(C=C2)Cl)NC(=O)C3=CC=CO3

Technology Process of Ethyl 4-(4-chlorophenyl)-2-(furan-2-carbonylamino)thiophene-3-carboxylate

There total 3 articles about Ethyl 4-(4-chlorophenyl)-2-(furan-2-carbonylamino)thiophene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dispiro ( bicyclo <3.3.1> nonan-3.1'-cyclobutan-3'.1'-cyclobutan )-dicarbonsaeure-(3'.3') (6240-35-3) → Dispiro-(bicyclo<3.3.1>nonan-3,1'-cyclobutan-3',1'-cyclobutan)-carbonsaeure-(3'') (6240-36-4)

Guidance literature:

at 200 ℃;

Reference yield:

3',3'-Bis-hydroxymethylspiro-(bicyclo<3.3.1>nonan-3,1'-cyclobutan)-ditosylat (6240-33-1) → Dispiro-(bicyclo<3.3.1>nonan-3,1'-cyclobutan-3',1'-cyclobutan)-carbonsaeure-(3'') (6240-36-4)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) Na, (ii) /BRN= 2683839/

2: KOH, MeOH

3: 200 °C

With methanol; potassium hydroxide;

Reference yield:

Dispiro ( bicyclo <3.3.1> nonan-3.1'-cyclobutan-3'.1'-cyclobutan )-dicarbonsaeure-(3'.3')-diethylester (6240-34-2) → Dispiro-(bicyclo<3.3.1>nonan-3,1'-cyclobutan-3',1'-cyclobutan)-carbonsaeure-(3'') (6240-36-4)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH, MeOH

2: 200 °C

With methanol; potassium hydroxide;

upstream raw materials:

Dispiro ( bicyclo <3.3.1> nonan-3.1'-cyclobutan-3'.1'-cyclobutan )-dicarbonsaeure-(3'.3')

3',3'-Bis-hydroxymethylspiro-(bicyclo<3.3.1>nonan-3,1'-cyclobutan)-ditosylat

Dispiro ( bicyclo <3.3.1> nonan-3.1'-cyclobutan-3'.1'-cyclobutan )-dicarbonsaeure-(3'.3')-diethylester

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