1H-Imidazole-2-carboxaldehyde, 1-((4-methoxy-3-nitrophenyl)methyl)-, (1-(3-nitro-4-(pentyloxy)phenyl)ethylidene)hydrazone

Base Information

Chemical Name:1H-Imidazole-2-carboxaldehyde, 1-((4-methoxy-3-nitrophenyl)methyl)-, (1-(3-nitro-4-(pentyloxy)phenyl)ethylidene)hydrazone
CAS No.:134221-19-5
Molecular Formula:C₂₅H₂₈N₆O₆
Molecular Weight:508.534
Hs Code.:

Synonyms:BRN 4833989;1H-Imidazole-2-carboxaldehyde, 1-((4-methoxy-3-nitrophenyl)methyl)-, (1-(3-nitro-4-(pentyloxy)phenyl)ethylidene)hydrazone;134221-19-5;C25H28N6O6;C25-H28-N6-O6;LS-78148

Suppliers and Price of 1H-Imidazole-2-carboxaldehyde, 1-((4-methoxy-3-nitrophenyl)methyl)-, (1-(3-nitro-4-(pentyloxy)phenyl)ethylidene)hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1H-Imidazole-2-carboxaldehyde, 1-((4-methoxy-3-nitrophenyl)methyl)-, (1-(3-nitro-4-(pentyloxy)phenyl)ethylidene)hydrazone

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:719.2°Cat760mmHg
Flash Point:388.8°C
Density:1.28g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:11
Exact Mass:508.20703263
Heavy Atom Count:37
Complexity:800

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCOC1=C(C=C(C=C1)C(=NN=CC2=NC=CN2CC3=CC(=C(C=C3)OC)[N+](=O)[O-])C)[N+](=O)[O-]
Isomeric SMILES:CCCCCOC1=C(C=C(C=C1)/C(=N\N=C\C2=NC=CN2CC3=CC(=C(C=C3)OC)[N+](=O)[O-])/C)[N+](=O)[O-]

Technology Process of 1H-Imidazole-2-carboxaldehyde, 1-((4-methoxy-3-nitrophenyl)methyl)-, (1-(3-nitro-4-(pentyloxy)phenyl)ethylidene)hydrazone

There total 4 articles about 1H-Imidazole-2-carboxaldehyde, 1-((4-methoxy-3-nitrophenyl)methyl)-, (1-(3-nitro-4-(pentyloxy)phenyl)ethylidene)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.4%

: 134221-17-3
4-amyloxy-3-nitroacetophenone

: 134221-15-1
[1-[1-(4-Methoxy-3-nitro-benzyl)-1H-imidazol-2-yl]-meth-(E)-ylidene]-hydrazine

: 134221-19-5
N-[1-[1-(4-Methoxy-3-nitro-benzyl)-1H-imidazol-2-yl]-meth-(E)-ylidene]-N'-[1-(3-nitro-4-pentyloxy-phenyl)-eth-(E)-ylidene]-hydrazine

Guidance literature:: In ethanol; for 5h;
DOI:10.1007/BF00766563

Reference yield:

: 5467-56-1
4-pentyloxyacetophenone

: 134221-19-5
N-[1-[1-(4-Methoxy-3-nitro-benzyl)-1H-imidazol-2-yl]-meth-(E)-ylidene]-N'-[1-(3-nitro-4-pentyloxy-phenyl)-eth-(E)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / HNO₃, H₂SO₄ / 2 h / -8 - -5 °C

2: 39.4 percent / ethanol / 5 h

With sulfuric acid; nitric acid; In ethanol;
DOI:10.1007/BF00766563

Reference yield:

: 134221-07-1
1-(4-methoxy-3-nitrobenzyl)imidazole-2-carboxaldehyde

: 134221-19-5
N-[1-[1-(4-Methoxy-3-nitro-benzyl)-1H-imidazol-2-yl]-meth-(E)-ylidene]-N'-[1-(3-nitro-4-pentyloxy-phenyl)-eth-(E)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / NH₂NH₂ / ethanol / 7 h / Heating

2: 39.4 percent / ethanol / 5 h

With hydrazine; In ethanol;
DOI:10.1007/BF00766563