9H-fluorene-9-thiol

Base Information

Chemical Name:9H-fluorene-9-thiol
CAS No.:19552-08-0
Molecular Formula:C13H10S
Molecular Weight:198.288
Hs Code.:2930909090
Mol file:19552-08-0.mol

Synonyms:Fluorenyl-(9)-mercaptan;9-Fluorenethiol;Fluorene-9-thiol;9-Fluorenthiol;9-Mercaptofluorene;Fluoren-9-thiol;9-Mercapto-fluoren;

Suppliers and Price of 9H-fluorene-9-thiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
9-Mercaptofluorene
1g
$ 193.00

American Custom Chemicals Corporation
9-MERCAPTOFLUORENE 95.00%
1G
$ 835.10

American Custom Chemicals Corporation
9-MERCAPTOFLUORENE 95.00%
250MG
$ 708.00

American Custom Chemicals Corporation
9-MERCAPTOFLUORENE 95.00%
50MG
$ 595.00

Total 9 raw suppliers

Chemical Property of 9H-fluorene-9-thiol

Chemical Property:

Vapor Pressure:0.000101mmHg at 25°C
Melting Point:103-107°C
Boiling Point:348.5°Cat760mmHg
Flash Point:169°C
PSA：38.80000
Density:1.22g/cm³
LogP:3.68620

Purity/Quality:

99%, ^*data from raw suppliers

9-Mercaptofluorene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:N
Statements: 50
Safety Statements: 61

MSDS Files:: SDS file from LookChem

Useful:

Uses This novel material is capable of self-assembly onto gold surfaces. The fluorene group is a precursor for the synthesis of luminophore materials that have longer lifespans and more efficient luminescence.

Technology Process of 9H-fluorene-9-thiol

There total 7 articles about 9H-fluorene-9-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 1689-64-1
9-Fluorenol

: 19552-08-0
9H-fluorene-9-thiol

Guidance literature:: With Lawessons reagent; In toluene; for 0.5h; Heating;

Reference yield:

: 64850-75-5
9H-fluoren-9-yl carbamimidothioate hydrobromide

: 19552-08-0
9H-fluorene-9-thiol

Guidance literature:: With sodium hydroxide; In water; at 70 ℃; for 3 - 5h;

Reference yield:

: 1940-57-4
9H-fluoren-9-yl bromide

: 19552-08-0
9H-fluorene-9-thiol

Guidance literature:: With potassium hydroxide; thiourea; Yield given. Multistep reaction; 1.) THF, reflux, 3 h, 2.) reflux, 4 h;
DOI:10.1016/S0040-4020(01)86322-5