[6aR,(+)]-9α-Ethenyl-2,6,6aβ,7,8,9,10,10aα-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole

Base Information

• Chemical Name: [6aR,(+)]-9α-Ethenyl-2,6,6aβ,7,8,9,10,10aα-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole
• CAS No.: 101968-75-6
• Molecular Formula: C21H24 N2
• Molecular Weight: 304.435
• Mol file: 101968-75-6.mol

Synonyms:Naphth[1,2,3-cd]indole,9-ethenyl-2,6,6a,7,8,9,10,10a-octahydro-10-isocyano-6,6,9-trimethyl-, [6aR-(6aa,9b,10b,10ab)]-; (+)-Hapalindole H;Hapalindole H

Chemical Property of [6aR,(+)]-9α-Ethenyl-2,6,6aβ,7,8,9,10,10aα-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole

Chemical Property:

• PSA: 28.15000
• LogP: 4.96820

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [6aR,(+)]-9α-Ethenyl-2,6,6aβ,7,8,9,10,10aα-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole

There total 50 articles about [6aR,(+)]-9α-Ethenyl-2,6,6aβ,7,8,9,10,10aα-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

<6aR*-(6aβ,9α,10α,10aα)>-10-formamido-2,6,6a,7,8,9,10,10a-octahydro-6,6,9-trimethyl-9-vinylnaphth<1,2,3-cd>indole (117184-32-4,124378-66-1,131616-24-5,131616-25-6,131616-34-7,131616-41-6) → (+/-)-hapalindole H (101968-75-6,106928-26-1,106928-30-7,124378-64-9,131616-21-2,131616-22-3,131616-26-7,131616-42-7)

Guidance literature:

With pyridine; trichlorophosphate; at -20 ℃; for 1h;

DOI:10.1016/S0040-4020(01)96007-7

Reference yield: 79.0%

<6aR*-(6aβ,9α,10α,10aβ)>-10-formamido-2,6,6a,7,8,9,10,10a-octahydro-6,6,9-trimethyl-9-vinylnaphth<1,2,3-cd>indole (117184-32-4,124378-66-1,131616-24-5,131616-25-6,131616-34-7,131616-41-6) → <6aR*-(6aβ,9α,10α,10aβ)>-2,6,6a,7,8,9,10,10a-octahydro-10-isocyano-6,6,9-trimethyl-9-vinylnaphth<1,2,3-cd>indole (101968-75-6,106928-26-1,106928-30-7,124378-64-9,131616-21-2,131616-22-3,131616-26-7,131616-42-7)

Guidance literature:

With pyridine; trichlorophosphate; at -20 ℃; for 0.666667h;

DOI:10.1016/S0040-4020(01)96007-7

Reference yield: 73.0%

<6aS*-(6aα,9α,10α,10aβ)>-10-formamido-2,6,6a,7,8,9,10,10a-octahydro-6,6,9-trimethyl-9-vinylnaphth<1,2,3-cd>indole (117184-32-4,124378-66-1,131616-24-5,131616-25-6,131616-34-7,131616-41-6) → (+/-)-hapalindole U (101968-75-6,106928-26-1,106928-30-7,124378-64-9,131616-21-2,131616-22-3,131616-26-7,131616-42-7)

Guidance literature:

With pyridine; trichlorophosphate; at -20 ℃; for 0.666667h;

DOI:10.1016/S0040-4020(01)96007-7

upstream raw materials:

<6aR*-(6aβ,9α,10α,10aα)>-10-formamido-2,6,6a,7,8,9,10,10a-octahydro-6,6,9-trimethyl-9-vinylnaphth<1,2,3-cd>indole

<6aR*-(6aβ,9α,10β,10aβ)>-2,6,6a,7,8,9,10,10a-octahydro-10-hydroxy-6,6,9-trimethyl-2-p-toluenesulfonyl-9-vinylnaphth<1,2,3-cd>indole

<6aR*-(6aβ,9α,10aα)>-2,6,6a,7,8,9,10,10a-octahydro-6,6,9-trimethyl-10-oxo-2-p-toluenesulfonyl-9-vinylnaphth<1,2,3-cd>indole

<6aR*-(6aβ,9α,10α,10aα)>-10-formamido-2,6,6a,7,8,9,10,10a-octahydro-6,6,9-trimethyl-2-p-toluenesulfonyl-9-vinylnaphth<1,2,3-cd>indole

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