CADMIUM IONOPHORE I

Base Information

• Chemical Name: CADMIUM IONOPHORE I
• CAS No.: 73487-00-0
• Molecular Formula: C₂₂H₄₄N₂O₂S₂
• Molecular Weight: 432.736
• Mol file: 73487-00-0.mol

Synonyms:ETH 1062;N,N,N',N'-Tetrabutyl-3,6-dioxaoctanedithioamide

Chemical Property of CADMIUM IONOPHORE I

Chemical Property:

• Vapor Pressure: 3.71E-10mmHg at 25°C
• Melting Point: 34-36 °C
• Boiling Point: 500.7°C at 760 mmHg
• Flash Point: 256.6°C
• PSA: 89.12000
• Density: 1.008g/cm³
• LogP: 5.47880
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

Cadmium ionophore I Selectophore? ^*data from reagent suppliers

Safty Information:

• Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of CADMIUM IONOPHORE I

There total 3 articles about CADMIUM IONOPHORE I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N,N,N',N'-Tetrabutyl-3,6-dioxaoctandiamid (70277-15-5) → N,N,N',N'-Tetrabutyl-3,6-dioxaoctandithioamid (73487-00-0)

Guidance literature:

With phosphorous (V) sulfide; In pyridine; at 90 ℃; for 24h;

DOI:10.1002/hlca.19800630121

Reference yield:

3,6-dioxasuberic acid (23243-68-7,39927-08-7) → N,N,N',N'-Tetrabutyl-3,6-dioxaoctandithioamid (73487-00-0)

Guidance literature:

Multi-step reaction with 3 steps

1: SOCl₂ / benzene; dimethylformamide / 24 h / Ambient temperature

2: 93 percent / benzene / 24 h / Ambient temperature

3: 91 percent / phosphorpentasulfide / pyridine / 24 h / 90 °C

With thionyl chloride; phosphorous (V) sulfide; In pyridine; N,N-dimethyl-formamide; benzene;

DOI:10.1002/hlca.19800630121

Reference yield:

3,6-dioxa-1,8-octanoyl dichloride (31255-09-1) → N,N,N',N'-Tetrabutyl-3,6-dioxaoctandithioamid (73487-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / benzene / 24 h / Ambient temperature

2: 91 percent / phosphorpentasulfide / pyridine / 24 h / 90 °C

With phosphorous (V) sulfide; In pyridine; benzene;

DOI:10.1002/hlca.19800630121

upstream raw materials:

N,N,N',N'-Tetrabutyl-3,6-dioxaoctandiamid

3,6-dioxasuberic acid

3,6-dioxa-1,8-octanoyl dichloride