3-amino-3-deoxyaltropyranosyl-3-amino-3-deoxyaltropyranoside

Base Information

• Chemical Name: 3-amino-3-deoxyaltropyranosyl-3-amino-3-deoxyaltropyranoside
• CAS No.: 110043-65-7
• Molecular Formula: C₁₂H₂₄N₂O₉
• Molecular Weight: 340.331
• Mol file: 110043-65-7.mol

Synonyms:3-amino-3-deoxyaltropyranosyl-3-amino-3-deoxyaltropyranoside

Chemical Property of 3-amino-3-deoxyaltropyranosyl-3-amino-3-deoxyaltropyranoside

Chemical Property:

• Vapor Pressure: 2.2E-23mmHg at 25°C
• Boiling Point: 711.4°Cat760mmHg
• Flash Point: 384.1°C
• PSA: 201.11000
• Density: 1.65g/cm³
• LogP: -4.06380

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-amino-3-deoxyaltropyranosyl-3-amino-3-deoxyaltropyranoside

There total 8 articles about 3-amino-3-deoxyaltropyranosyl-3-amino-3-deoxyaltropyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-acetamido-3-deoxy-α-D-altropyranosyl 3-acetamido-3-deoxy-α-D-altropyranoside (109986-74-5) → 3-amino-3-deoxy-α-D-altropyranosyl 3-amino-3-deoxy-α-D-altropyranoside (110043-65-7)

Guidance literature:

With barium dihydroxide; In water; for 1.5h; Heating;

DOI:10.1016/0008-6215(86)85060-1

Reference yield:

3-azido-3-deoxy-α-D-altropyranosyl 3-azido-3-deoxy-α-D-altropyranoside (109986-70-1) → 3-amino-3-deoxy-α-D-altropyranosyl 3-amino-3-deoxy-α-D-altropyranoside (110043-65-7)

Guidance literature:

With cyclohexa-1,4-diene; palladium on activated charcoal; In methanol; water; for 0.5h; Yield given; Ambient temperature;

DOI:10.1016/0008-6215(86)85060-1

Reference yield:

C26H28N6O9 (40094-11-9) → 3-amino-3-deoxy-α-D-altropyranosyl 3-amino-3-deoxy-α-D-altropyranoside (110043-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 52 percent / 80percent acetic acid / 0.75 h / Heating

2: 1,4-cyclohexadiene / 10percent Pd/C / H₂O; methanol / 0.5 h / Ambient temperature

With cyclohexa-1,4-diene; acetic acid; palladium on activated charcoal; In methanol; water;

DOI:10.1016/0008-6215(86)85060-1

upstream raw materials:

3-azido-3-deoxy-α-D-altropyranosyl 3-azido-3-deoxy-α-D-altropyranoside

Acetic acid (2R,3S,4R,5S,6R)-5-acetoxy-6-acetoxymethyl-4-acetylamino-2-((2R,3S,4R,5S,6R)-3,5-diacetoxy-6-acetoxymethyl-4-acetylamino-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

3-acetamido-3-deoxy-α-D-altropyranosyl 3-acetamido-3-deoxy-α-D-altropyranoside

C₂₆H₂₈N₆O₉

Refernces