5-methoxytryptoline

Base Information

Chemical Name:5-methoxytryptoline
CAS No.:30439-19-1
Molecular Formula:C₁₂H₁₄N₂O
Molecular Weight:202.256
Hs Code.:2933990090
Mol file:30439-19-1.mol

Synonyms:5-Methoxytryptoline

Suppliers and Price of 5-methoxytryptoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
2,3,4,9-tetrahydro-5-methoxy-1H-Pyrido[3,4-b]indole 97.00%
5G
$ 6840.00

AccelPharmtech
2,3,4,9-tetrahydro-5-methoxy-1H-Pyrido[3,4-b]indole 97.00%
1G
$ 3960.00

Total 3 raw suppliers

Chemical Property of 5-methoxytryptoline

Chemical Property:

Vapor Pressure:3.03E-06mmHg at 25°C
Boiling Point:388.6°Cat760mmHg
Flash Point:188.8°C
PSA：37.05000
Density:1.198g/cm³
LogP:2.15100

Purity/Quality:

98% ^*data from raw suppliers

2,3,4,9-tetrahydro-5-methoxy-1H-Pyrido[3,4-b]indole 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-methoxytryptoline

There total 7 articles about 5-methoxytryptoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.2%

: 6000-59-5,1152495-30-1
glyoxalic acid monohydrate

: 74217-56-4,26579-75-9
4-methoxytryptamine hydrochloride

: 30439-19-1
5-methoxy-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

Guidance literature:: In water; for 1h; Reflux;
DOI:10.1021/jm800689g

Reference yield: 49.0%

: 74217-56-4,26579-75-9
4-methoxytryptamine hydrochloride

: 298-12-4
Glyoxilic acid

: 30439-19-1
5-methoxy-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

Guidance literature:: In water; for 1h; Heating;
DOI:10.1002/jhet.5570190428

Reference yield:

: 4837-88-1
6-methoxy-2-nitrotoluene

: 30439-19-1
5-methoxy-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) pyrrolidine; 2.) 85percent N₂H₄ / 2.) Raney Ni / 1.) DMF, 125 deg C, 3 h; 2.) methanol, 50-60 deg C, 3 h

2: 56 percent / trifluoroacetic acid / 0.5 h / Ambient temperature

3: 65 percent / LiAlH₄; HCl / tetrahydrofuran / 0.25 h / Heating

4: 49 percent / H₂O / 1 h / Heating

With pyrrolidine; hydrogenchloride; lithium aluminium tetrahydride; hydrazine hydrate; nickel; In tetrahydrofuran; water; trifluoroacetic acid;
DOI:10.1002/jhet.5570190428