2,7-Di-tert-butylthiepin, 4,5-dimethyl-

Base Information

Chemical Name:2,7-Di-tert-butylthiepin, 4,5-dimethyl-
CAS No.:84477-45-2
Molecular Formula:C₁₆H₂₆S
Molecular Weight:250.448
Hs Code.:
DSSTox Substance ID:DTXSID60233453

Synonyms:2,7-Di-tert-butylthiepin, 4,5-dimethyl-;84477-45-2;2,7-Di-tert-butylthiepin,4,5-dimethyl-;DTXSID60233453

Suppliers and Price of 2,7-Di-tert-butylthiepin, 4,5-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,7-Di-tert-butylthiepin, 4,5-dimethyl-

Chemical Property:

Vapor Pressure:0.00035mmHg at 25°C
Boiling Point:329°Cat760mmHg
Flash Point:139.9°C
Density:0.934g/cm³
XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:250.17552200
Heavy Atom Count:17
Complexity:354

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(SC(=C1)C(C)(C)C)C(C)(C)C)C

Technology Process of 2,7-Di-tert-butylthiepin, 4,5-dimethyl-

There total 4 articles about 2,7-Di-tert-butylthiepin, 4,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 84477-48-5
2,7-Di-tert-butyl-4-methoxymethyl-5-methyl-thiepine

: 84477-45-2
2,7-di-tert-butyl-4,5-dimethylthiepine

Guidance literature:: With diisobutylaluminium hydride;

Reference yield:

: 71951-58-1
2,7-Di-tert-butyl-5-methyl-4-thiepincarbonsaeureethylester

: 84477-45-2
2,7-di-tert-butyl-4,5-dimethylthiepine

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄

2: trihexylphosphine, CCl₄

3: LiAlH₄ / diethyl ether

With tetrachloromethane; lithium aluminium tetrahydride; trihexylphosphine; In diethyl ether;
DOI:10.1246/cl.1982.1843

Reference yield:

: 84477-44-1
2,7-di-tert-butyl-4-methyl-5-hydroxymethylthiepin

: 84477-45-2
2,7-di-tert-butyl-4,5-dimethylthiepine

Guidance literature:: Multi-step reaction with 2 steps

1: trihexylphosphine, CCl₄

2: LiAlH₄ / diethyl ether

With tetrachloromethane; lithium aluminium tetrahydride; trihexylphosphine; In diethyl ether;
DOI:10.1246/cl.1982.1843