10-(3-Diethylaminopropyl)-10H-pyrido[3,2-b][1,4]benzothiazine

Base Information

• Chemical Name: 10-(3-Diethylaminopropyl)-10H-pyrido[3,2-b][1,4]benzothiazine
• CAS No.: 67465-67-2
• Molecular Formula: C18H23N3S
• Molecular Weight: 313.4603
• Mol file: 67465-67-2.mol

Synonyms:D 209;10H-Pyrido(3,2-b)(1,4)benzothiazine,10-(3-(diethylamino)propyl);10-(3-(Diethylamino)propyl)-10H-pyrido(3,2-b)(1,4)benzothiazine;

Chemical Property of 10-(3-Diethylaminopropyl)-10H-pyrido[3,2-b][1,4]benzothiazine

Chemical Property:

• Vapor Pressure: 1.88E-08mmHg at 25°C
• Boiling Point: 454.6°Cat760mmHg
• Flash Point: 228.7°C
• PSA: 44.67000
• Density: 1.13g/cm³
• LogP: 4.48120

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 10-(3-Diethylaminopropyl)-10H-pyrido[3,2-b][1,4]benzothiazine

There total 3 articles about 10-(3-Diethylaminopropyl)-10H-pyrido[3,2-b][1,4]benzothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(phenylamino)pyridine (6631-37-4) → 10-<3-Diaethylamino-propyl>-4-aza-phenothiazin (67465-67-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfur, I₂ / 250 - 335 °C

2: NaNH₂

With iodine; sulfur; sodium amide;

Reference yield:

1-azaphenothiazine (261-96-1) + 3-diethylaminopropyl chloride (104-77-8) → 10-<3-Diaethylamino-propyl>-4-aza-phenothiazin (67465-67-2)

Guidance literature:

With sodium amide;

Reference yield:

→ 10-<3-Diaethylamino-propyl>-4-aza-phenothiazin (67465-67-2)

Guidance literature:

Thiophenylpyridylamin, 1. NaNH2, Toluol, Rueckfluss, 2. 3(?)-Diaethylamino-propylchlorid, Toluol, Rueckfluss;

upstream raw materials:

1-azaphenothiazine

3-diethylaminopropyl chloride

2-(phenylamino)pyridine

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