5-Benzoyluridine

Base Information

Chemical Name:5-Benzoyluridine
CAS No.:85372-91-4
Molecular Formula:C16H16 N2 O7
Molecular Weight:348.312
Hs Code.:
European Community (EC) Number:286-748-0
DSSTox Substance ID:DTXSID60234546
Nikkaji Number:J310.323D
Wikidata:Q83116346
Mol file:85372-91-4.mol

Synonyms:5-Benzoyluridine;85372-91-4;EINECS 286-748-0;SCHEMBL7101690;DTXSID60234546;ANFJQBUYDIHRPP-BPGGGUHBSA-N;NS00038887

Suppliers and Price of 5-Benzoyluridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5-Benzoyluridine

Chemical Property:

PSA：142.11000
Density:1.577g/cm³
LogP:-1.20860
Storage Temp.:-20°C
XLogP3:-0.4
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:348.09575085
Heavy Atom Count:25
Complexity:599

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C2=CN(C(=O)NC2=O)C3C(C(C(O3)CO)O)O
Isomeric SMILES:C1=CC=C(C=C1)C(=O)C2=CN(C(=O)NC2=O)[C@H]3[C@@H]([C@@H]([C@H](O3)CO)O)O

Technology Process of 5-Benzoyluridine

There total 11 articles about 5-Benzoyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 85372-86-7
5-benzoyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

: 85372-91-4
5-benzoyluridine

Guidance literature:: With trifluoroacetic acid; for 72h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96481-6

Reference yield: 82.0%

: 110522-95-7
5-Benzoyl-1-[(2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

: 85372-91-4
5-benzoyluridine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95656-9

Reference yield:

: 80614-78-4
2',3'-O-isopropylidene-5'-O-methoxymethyl-uridine

: 85372-91-4
5-benzoyluridine

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / 5percent Rh on alumina / methanol

2: 1.) LDA / 1.) THF, -70 deg C; 2.) THF, -70 deg C, 1 h

3: 1.) PhSeCl-pyridine; 2.) 30percent H₂O₂ / 1.) CH₂Cl₂, 0 deg C, rt overnight; 2.) CH₂Cl₂, 0 deg C, 2 h

4: 84.3 percent / 50percent aqueous trifluoroacetic acid

With pyridine; Phenylselenyl chloride; hydrogen; dihydrogen peroxide; trifluoroacetic acid; lithium diisopropyl amide; rhodium on alumina; In methanol;
DOI:10.1248/cpb.30.4589