(2R)-1-(furan-3-yl)-4,4,7a-trimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-2-yl acetate

Base Information

Chemical Name:(2R)-1-(furan-3-yl)-4,4,7a-trimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-2-yl acetate
CAS No.:124098-15-3
Molecular Formula:C₁₈H₂₄O₃
Molecular Weight:288.387
Hs Code.:

Synonyms:1H-Inden-2-ol,1-(3-furanyl)-2,4,5,6,7,7a-hexahydro-4,4,7a-trimethyl-, acetate, (2a,3b,3ab)- (9CI); 1H-Inden-2-ol,1-(3-furanyl)-2,4,5,6,7,7a-hexahydro-4,4,7a-trimethyl-, acetate, (2a,3b,3ab)-(?à)-

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-1-(furan-3-yl)-4,4,7a-trimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-2-yl acetate

Chemical Property:

Vapor Pressure:6.6E-05mmHg at 25°C
Boiling Point:344.4°Cat760mmHg
Flash Point:162.1°C
Density:1.09g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2R)-1-(furan-3-yl)-4,4,7a-trimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-2-yl acetate

There total 5 articles about (2R)-1-(furan-3-yl)-4,4,7a-trimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 124098-16-4
(1RS,2RS,7aSR)-1-(3-furyl)-4,4,7a-trimethyl-1,4,5,6,7,7a-hexahydro-2H-inden-2-ol

: 108-24-7
acetic anhydride

: 124098-15-3
(1RS,2RS,7aSR)-2-acetoxy-1-(3-furyl)-4,4,7a-trimethyl-1,4,5,6,7,7a-hexahydro-2H-indene

Guidance literature:: With pyridine; for 3h; Ambient temperature;
DOI:10.1021/jo00291a048

Reference yield:

: 124070-88-8,860003-90-3
(E)-1-(3-furyl)-2-nitro-1-propene

: 124098-15-3
(1RS,2RS,7aSR)-2-acetoxy-1-(3-furyl)-4,4,7a-trimethyl-1,4,5,6,7,7a-hexahydro-2H-indene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) TiCl₄ 2.) H₂O / 1.) CH₂Cl₂, -78 deg C 2.) H₂O, 2h

2: 64 percent / KOH / ethanol / 0.67 h / Heating

3: 97 percent / LiAlH₄ / diethyl ether / 3 h / 0 °C

4: 93 percent / pyridine / 3 h / Ambient temperature

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; water; titanium tetrachloride; In diethyl ether; ethanol;
DOI:10.1021/jo00291a048

Reference yield:

: 124070-94-6
(1'RS,2SR)-2,6,6-trimethyl-2-<1'-(3-furyl)-2-oxopropyl>cyclohexanone

: 124098-15-3
(1RS,2RS,7aSR)-2-acetoxy-1-(3-furyl)-4,4,7a-trimethyl-1,4,5,6,7,7a-hexahydro-2H-indene

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / KOH / ethanol / 0.67 h / Heating

2: 97 percent / LiAlH₄ / diethyl ether / 3 h / 0 °C

3: 93 percent / pyridine / 3 h / Ambient temperature

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; In diethyl ether; ethanol;
DOI:10.1021/jo00291a048