7-Oxo-1,4,5,6-tetraphenyl-3-(phenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

Base Information

Chemical Name:7-Oxo-1,4,5,6-tetraphenyl-3-(phenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate
CAS No.:6814-93-3
Molecular Formula:C39H28NO4-
Molecular Weight:574.6445
Hs Code.:
DSSTox Substance ID:DTXSID10411027

Synonyms:6814-93-3;DTXSID10411027;7-Oxo-1,4,5,6-tetraphenyl-3-(phenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Oxo-1,4,5,6-tetraphenyl-3-(phenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

Chemical Property:

Vapor Pressure:1.13E-26mmHg at 25°C
Boiling Point:795.3°C at 760 mmHg
Flash Point:434.8°C
XLogP3:6.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:574.20183337
Heavy Atom Count:44
Complexity:1110

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C3(C(C(C2(C3=O)C4=CC=CC=C4)C(=O)NC5=CC=CC=C5)C(=O)[O-])C6=CC=CC=C6)C7=CC=CC=C7

Technology Process of 7-Oxo-1,4,5,6-tetraphenyl-3-(phenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

There total 1 articles about 7-Oxo-1,4,5,6-tetraphenyl-3-(phenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 709-50-2
methyl beta-D-glucopyranoside

: 98-80-6
phenylboronic acid

: 6814-93-3
methyl β-D-glucopyranoside 4,6-phenylboronate

Guidance literature:: at 90 ℃; for 0.25h; under 0.1 Torr;
DOI:10.1002/chem.202001970

Reference yield:

: 6814-93-3
methyl β-D-glucopyranoside 4,6-phenylboronate

: methyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→3)-β-D-glucopyranosyl-(1→3)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate / 1,2-dimethoxyethane / 1.5 h / Inert atmosphere; Molecular sieve

2: Amberlite IRA 743 / methanol; dichloromethane / 20 °C / Inert atmosphere

With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; In methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1002/ejoc.201300723

Reference yield:

: 6814-93-3
methyl β-D-glucopyranoside 4,6-phenylboronate

: methyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1→3)-2,4,6-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate / 1,2-dimethoxyethane / 1.5 h / Inert atmosphere; Molecular sieve

2: Amberlite IRA 743 / methanol; dichloromethane / 20 °C / Inert atmosphere

3: pyridine

With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; In pyridine; methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1002/ejoc.201300723