4,5-Dimethoxy-9,10-dihydrophenanthrene

Base Information

Chemical Name:4,5-Dimethoxy-9,10-dihydrophenanthrene
CAS No.:10127-53-4
Molecular Formula:C₁₆H₁₆O₂
Molecular Weight:240.302
Hs Code.:
NSC Number:172564
DSSTox Substance ID:DTXSID20305903
Nikkaji Number:J921.314G
Wikidata:Q82052709
Mol file:10127-53-4.mol

Synonyms:4,5-dimethoxy-9,10-dihydrophenanthrene;10127-53-4;NSC172564;DTXSID20305903;NSC-172564

Suppliers and Price of 4,5-Dimethoxy-9,10-dihydrophenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4,5-Dimethoxy-9,10-dihydrophenanthrene

Chemical Property:

Vapor Pressure:3.45E-06mmHg at 25°C
Boiling Point:398.2°Cat760mmHg
Flash Point:166°C
Density:1.122g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:240.115029749
Heavy Atom Count:18
Complexity:250

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC2=C1C3=C(CC2)C=CC=C3OC

Technology Process of 4,5-Dimethoxy-9,10-dihydrophenanthrene

There total 2 articles about 4,5-Dimethoxy-9,10-dihydrophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 15330-99-1,38197-29-4,38197-30-7
2,2'-bis(bromomethyl)-6,6'-dimethoxy-1,1'-biphenyl

: 10127-53-4
4,5-dimethoxy-9,10-dihydrophenanthrene

Guidance literature:: With magnesium; ethylene dibromide; In diethyl ether; Heating;

Reference yield:

: 591-51-5
phenyllithium

: 10127-53-4
4,5-dimethoxy-9,10-dihydrophenanthrene

Guidance literature:: With diethyl ether;
DOI:10.1039/jr9510003072

Reference yield:

: 10127-53-4
4,5-dimethoxy-9,10-dihydrophenanthrene

: 10117-15-4
5-Hydroxy-1,4-phenanthrenchinon

Guidance literature:: Multi-step reaction with 3 steps

1: sulfur / 225 °C

2: Py*HCl / 210 °C

3: (KO₃S)2NO, KH₂PO₄ / acetone

With potassium dihydrogenphosphate; potassium nitrososulfonate; pyridine hydrochloride; sulfur; In acetone;
DOI:10.1021/jo01277a015