1,4-Phenanthrenedione, 6,7-dimethoxy-

Base Information

• Chemical Name: 1,4-Phenanthrenedione, 6,7-dimethoxy-
• CAS No.: 63216-09-1
• Molecular Formula: C₁₆H₁₂O₄
• Molecular Weight: 268.269
• DSSTox Substance ID: DTXSID60212581
• Nikkaji Number: J834.383G
• Wikidata: Q83087723

Synonyms:1,4-Phenanthrenedione, 6,7-dimethoxy-;63216-09-1;6,7-dimethoxyphenanthrene-1,4-dione;DTXSID60212581

Chemical Property of 1,4-Phenanthrenedione, 6,7-dimethoxy-

Chemical Property:

• Vapor Pressure: 1.66E-08mmHg at 25°C
• Boiling Point: 456.1°Cat760mmHg
• Flash Point: 205.2°C
• Density: 1.31g/cm³
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 268.07355886
• Heavy Atom Count: 20
• Complexity: 442

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=C2C(=C1)C=CC3=C2C(=O)C=CC3=O)OC

Technology Process of 1,4-Phenanthrenedione, 6,7-dimethoxy-

There total 6 articles about 1,4-Phenanthrenedione, 6,7-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2-(3,4-dimethoxyphenyl)-1-(3,6-dioxo-1,4-cyclohexadienyl)ethanol (221876-35-3) → 6,7-dimethoxy-1,4-phenanthrenequinone (63216-09-1)

Guidance literature:

With tin(IV) chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at -78 - 20 ℃;

DOI:10.1021/jo981352f

Reference yield: 31.0%

3,4-dimethoxystyrene (6380-23-0) + p-benzoquinone (106-51-4) → 6,7-dimethoxy-1,4-phenanthrenequinone (63216-09-1)

Guidance literature:

With trichloroacetic acid; In toluene; at 100 ℃;

DOI:10.1021/jo01300a064

Reference yield:

3,4-dimethoxystyrene (6380-23-0) + (+/-)-2-(p-tolylsulfinyl)-1,4-benzoquinone → 6,7-dimethoxy-1,4-phenanthrenequinone (63216-09-1) + 6,7-Dimethoxy-3-(toluene-4-sulfinyl)-phenanthrene-1,4-dione + 6,7-Dimethoxy-2-(toluene-4-sulfinyl)-phenanthrene-1,4-dione

Guidance literature:

In toluene; at 110 ℃; for 24h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(97)00505-4

upstream raw materials:

3,4-dimethoxystyrene

p-benzoquinone

2-(3,4-dimethoxyphenyl)-1-(3,6-dioxo-1,4-cyclohexadienyl)ethanol

1-methoxy-1,3-cyclohexadiene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 63216-09-1 6,7-dimethoxyphenanthrene-1,4-dione

Send

Send

Metric Ton KG G Pound L ML

Send

Send