5-[(2,5-Dimethoxyphenyl)methylidene]-1-phenyl-1,3-diazinane-2,4,6-trione

Base Information

Chemical Name:5-[(2,5-Dimethoxyphenyl)methylidene]-1-phenyl-1,3-diazinane-2,4,6-trione
CAS No.:5809-92-7
Molecular Formula:C19H16N2O5
Molecular Weight:190.242
Hs Code.:
DSSTox Substance ID:DTXSID20361524

Synonyms:5809-92-7;5-[(2,5-dimethoxyphenyl)methylidene]-1-phenyl-1,3-diazinane-2,4,6-trione;CBMicro_034277;DTXSID20361524

Suppliers and Price of 5-[(2,5-Dimethoxyphenyl)methylidene]-1-phenyl-1,3-diazinane-2,4,6-trione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 5-[(2,5-Dimethoxyphenyl)methylidene]-1-phenyl-1,3-diazinane-2,4,6-trione

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.339g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:352.10592162
Heavy Atom Count:26
Complexity:597

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)OC)C=C2C(=O)NC(=O)N(C2=O)C3=CC=CC=C3

Technology Process of 5-[(2,5-Dimethoxyphenyl)methylidene]-1-phenyl-1,3-diazinane-2,4,6-trione

There total 4 articles about 5-[(2,5-Dimethoxyphenyl)methylidene]-1-phenyl-1,3-diazinane-2,4,6-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 105-38-4
vinyl propionate

: 90-27-7
2-Phenylbutyric acid

: 5809-92-7
(+/-)-2-phenylbutyric acid vinyl ester

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 80 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.202100760

Reference yield: 47.0%

: 20452-67-9
phenylethylketene

: 675825-21-5
Lithium enolate of the acetaldehyde

: 5809-92-7
(+/-)-2-phenylbutyric acid vinyl ester

Guidance literature:: In tetrahydrofuran;
DOI:10.1021/jo00298a047

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 90-27-7
2-Phenylbutyric acid

: 5809-92-7
(+/-)-2-phenylbutyric acid vinyl ester

Guidance literature:: With sulfuric acid; mercury(II) diacetate; Yield given; Multistep reaction; 1.) room temperature, 30 min, 2.) reflux, 6 h;
DOI:10.1021/jo981780l