6-Oxabicyclo[3.2.2]nonan-7-one

Base Information

Chemical Name:6-Oxabicyclo[3.2.2]nonan-7-one
CAS No.:27873-57-0
Molecular Formula:C₈H₁₂O₂
Molecular Weight:140.182
Hs Code.:
NSC Number:119484
DSSTox Substance ID:DTXSID40297937
Mol file:27873-57-0.mol

Synonyms:27873-57-0;6-oxabicyclo[3.2.2]nonan-7-one;NSC119484;DTXSID40297937;9-oxabicyclo[3.2.2]nonan-8-one;NSC-119484

Suppliers and Price of 6-Oxabicyclo[3.2.2]nonan-7-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 6-Oxabicyclo[3.2.2]nonan-7-one

Chemical Property:

Vapor Pressure:0.0107mmHg at 25°C
Boiling Point:262.8°Cat760mmHg
Flash Point:103.8°C
Density:1.093g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:140.083729621
Heavy Atom Count:10
Complexity:153

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2CCC(C1)OC2=O

Technology Process of 6-Oxabicyclo[3.2.2]nonan-7-one

There total 7 articles about 6-Oxabicyclo[3.2.2]nonan-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 63048-50-0
(1α,4α,5α)-4-(phenylseleno)-6-oxabicyclo<3.2.2>nonan-7-one

: 27873-57-0
6-Oxabicyclo<3.2.2>nonan-7-on

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 110 ℃; for 1h;
DOI:10.1016/S0040-4020(01)93285-5

Reference yield:

: 55679-31-7
bicyclo<3.2.1>octan-8-one

: 27873-57-0
6-Oxabicyclo<3.2.2>nonan-7-on

Guidance literature:: With dihydrogen peroxide; fluorous reverse-phase silica gel-Sn[N(SO₂C₈F₁₇)2]4; In water; at 25 ℃; for 16h;
DOI:10.1016/j.tetlet.2003.09.183

Reference yield:

: 502-42-1
cycloheptanone

: 27873-57-0
6-Oxabicyclo<3.2.2>nonan-7-on

Guidance literature:: Multi-step reaction with 3 steps

1: NaHSO₃, KCN / H₂O / 2 h / 25 °C

2: 19 percent / glacial acetic acid, conc. HCl / 3 h

3: FSO₃-SO₂ / 1.) -70 deg C, 2.) -20 deg c then 0 deg C

With hydrogenchloride; potassium cyanide; sulfur dioxide; fluorosulphonic acid; sodium hydrogensulfite; acetic acid; In water;