HEXAFLUOROGLUTARAMIDE

Base Information

• Chemical Name: HEXAFLUOROGLUTARAMIDE
• CAS No.: 507-68-6
• Molecular Formula: C5H4 F6 N2 O2
• Molecular Weight: 238.089
• Hs Code.: 2924199090
• Mol file: 507-68-6.mol

Synonyms:Glutaramide,2,2,3,3,4,4-hexafluoro- (7CI,8CI); NSC 71120

Chemical Property of HEXAFLUOROGLUTARAMIDE

Chemical Property:

• Vapor Pressure: 0.000246mmHg at 25°C
• Melting Point: 209-211°C
• Boiling Point: 324.4°Cat760mmHg
• PKA: 12.71±0.50(Predicted)
• Flash Point: 150°C
• PSA: 86.18000
• Density: 1.636g/cm³
• LogP: 1.26350

Purity/Quality:

98%min ^*data from raw suppliers

Hexafluoroglutaramide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of HEXAFLUOROGLUTARAMIDE

There total 7 articles about HEXAFLUOROGLUTARAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl perfluoroglutarate (424-40-8) → hexafluoroglutaramide (507-68-6)

Guidance literature:

With diethyl ether; ammonia;

DOI:10.1021/ja01147a064

Reference yield:

1-chloro-5H-decafluoro-pentane (355-29-3) → hexafluoroglutaramide (507-68-6)

Guidance literature:

Multi-step reaction with 4 steps

1: (FSO₂O)2

2: ClOSO₂F, HSO₃F, SbF₅

3: KF / bis-(2-methoxy-ethyl) ether

4: NH₃

With potassium fluoride; chlorine fluorosulfate; bis(fluorosulfuryl) peroxide; ammonia; antimony pentafluoride; fluorosulphonic acid; In diethylene glycol dimethyl ether;

Reference yield:

1,5-Dichloro-1,1,2,2,3,3,4,4,5,5-decafluoro-pentane → hexafluoroglutaramide (507-68-6)

Guidance literature:

Multi-step reaction with 3 steps

1: ClOSO₂F, (FSO₂O)2, HSO₃F, SbF₅

2: KF / bis-(2-methoxy-ethyl) ether

3: NH₃

With potassium fluoride; chlorine fluorosulfate; bis(fluorosulfuryl) peroxide; ammonia; antimony pentafluoride; fluorosulphonic acid; In diethylene glycol dimethyl ether;

upstream raw materials:

diethyl perfluoroglutarate

hexafluoroglutaryl fluoride

1-chloro-5H-decafluoro-pentane

Downstream raw materials:

hexafluoro-glutaronitrile

Refernces

• 1、 Rapkin, A. I.,Zabolot-skikh, V. F.,Kochanov, A. S.,Tiunov, A. V.,Zhirnov, O. M.. "Use of Perfluoroalkylfluorosulfonates for Synthesizing Organofluorine Compounds". . p. 133 - 134. Retrieved 2007/10/03.