2-[2-(4-Methoxyphenyl)-2-oxoethyl]-1,3-cyclohexanedione

Base Information

• Chemical Name: 2-[2-(4-Methoxyphenyl)-2-oxoethyl]-1,3-cyclohexanedione
• CAS No.: 39992-64-8
• Molecular Formula: C₁₅H₁₆O₄
• Molecular Weight: 260.29
• Mol file: 39992-64-8.mol

Synonyms:2-p-Methoxyphenacylcyclohexane-1,3-dione;1,3-Cyclohexanedione,2-(2-(4-methoxyphenyl)-2-oxoethyl);1,3-Cyclohexanedione,2-p-methoxyphenacyl;

Chemical Property of 2-[2-(4-Methoxyphenyl)-2-oxoethyl]-1,3-cyclohexanedione

Chemical Property:

• Vapor Pressure: 6.2E-09mmHg at 25°C
• Boiling Point: 468°Cat760mmHg
• Flash Point: 210.2°C
• PSA: 60.44000
• Density: 1.18g/cm³
• LogP: 2.20630

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[2-(4-Methoxyphenyl)-2-oxoethyl]-1,3-cyclohexanedione

There total 1 articles about 2-[2-(4-Methoxyphenyl)-2-oxoethyl]-1,3-cyclohexanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

1,3-cylohexanedione (504-02-9) + 2-Bromo-4'-methoxyacetophenone (2632-13-5) → 2-p-Methoxyphenacylcyclohexane-1,3-dione (39992-64-8)

Guidance literature:

With potassium hydroxide; In various solvent(s); Ambient temperature;

DOI:10.1007/BF00765625

Reference yield: 63.0%

2-p-Methoxyphenacylcyclohexane-1,3-dione (39992-64-8) + aniline (62-53-3) → 1-Phenyl-2-p-methoxyphenyl-4-oxo-4,5,6,7-tetrahydroindole (76410-25-8)

Guidance literature:

In acetic acid; for 0.666667h; Heating;

DOI:10.1007/BF00765625

Reference yield: 52.0%

2-p-Methoxyphenacylcyclohexane-1,3-dione (39992-64-8) + isopropylamine (75-31-0) → 1-isopropyl-2-(4-methoxyphenyl)-1,5,6,7-tetrahydro-4H-indol-4-one (76410-26-9)

Guidance literature:

In acetic acid; for 0.666667h; Heating;

DOI:10.1007/BF00765625

upstream raw materials:

1,3-cylohexanedione

2-Bromo-4'-methoxyacetophenone

Downstream raw materials:

1-isopropyl-2-(4-methoxyphenyl)-1,5,6,7-tetrahydro-4H-indol-4-one

1-Phenyl-2-p-methoxyphenyl-4-oxo-4,5,6,7-tetrahydroindole

1-Isopropyl-2-p-methoxyphenyl-4-hydroxyindole

1-Phenyl-2-p-methoxyphenyl-4-hydroxyindole