6-hydroxy-methyl 1'-epiacarviosin

Base Information

• Chemical Name: 6-hydroxy-methyl 1'-epiacarviosin
• CAS No.: 101144-24-5
• Molecular Formula: C14H25 N O9
• Molecular Weight: 351.35
• Mol file: 101144-24-5.mol

Synonyms:a-D-Glucopyranoside, methyl4-deoxy-4-[[4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexen-1-yl]amino]-,[1R-(1a,4b,5a,6b)]-

Chemical Property of 6-hydroxy-methyl 1'-epiacarviosin

Chemical Property:

• Boiling Point: 634.4°Cat760mmHg
• Flash Point: 337.5°C
• PSA: 172.10000
• Density: 1.57g/cm³
• LogP: -4.19550

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-hydroxy-methyl 1'-epiacarviosin

There total 12 articles about 6-hydroxy-methyl 1'-epiacarviosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl 4-deoxy-4-<(1R)-(1,5/4,6)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>amino-α-D-glucopyranoside 4',7':5',6'-di-O-isopropylidene derivative (131922-33-3,140148-04-5) → methyl 4-deoxy-4-<(1R)-(1,5/4,6)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>amino-α-D-glucopyranoside (101144-24-5)

Guidance literature:

With acetic acid; at 60 ℃; for 2h;

DOI:10.1016/0008-6215(92)80025-V

Reference yield:

Benzoic acid 4,5,6-triacetoxy-3-((2S,3R,4S,5R,6S)-4,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-cyclohex-1-enylmethyl ester (141232-09-9) → (1S,2R,3S,6R)-6-((2S,3S,4S,5R,6S)-4,5-Dihydroxy-2-hydroxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-4-hydroxymethyl-cyclohex-4-ene-1,2,3-triol (89859-74-5,89920-25-2,101144-22-3,101144-24-5,141316-51-0) + (1R,2S,3R,6S)-6-((2S,3S,4S,5R,6S)-4,5-Dihydroxy-2-hydroxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-4-hydroxymethyl-cyclohex-4-ene-1,2,3-triol (89859-74-5,89920-25-2,101144-22-3,101144-24-5,141316-51-0)

Guidance literature:

With sodium methylate; In methanol; for 0.666667h; Ambient temperature;

DOI:10.1016/S0008-6215(00)90465-8

Reference yield:

Benzoic acid 4,5,6-triacetoxy-3-((2S,3R,4S,5R,6S)-4,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-cyclohex-1-enylmethyl ester (141232-09-9) → (1S,2R,3S,6R)-6-((2S,3S,4S,5R,6S)-4,5-Dihydroxy-2-hydroxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-4-hydroxymethyl-cyclohex-4-ene-1,2,3-triol (89859-74-5,89920-25-2,101144-22-3,101144-24-5,141316-51-0) + (1R,2S,3R,6S)-6-((2S,3S,4S,5R,6S)-4,5-Dihydroxy-2-hydroxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-4-hydroxymethyl-cyclohex-4-ene-1,2,3-triol (89859-74-5,89920-25-2,101144-22-3,101144-24-5,141316-51-0)

Guidance literature:

With sodium methylate; In methanol; for 0.666667h; Ambient temperature;

DOI:10.1016/S0008-6215(00)90465-8

upstream raw materials:

Methyl-4-amino-4-deoxy-α-D-glucopyranoside

D,L-(1,2,4/3)-3,4-di-O-acetyl-1,2-anhydro-5-benzoyloxymethyl-5-cyclohexene-1,2,3,4,-tetrol

methyl 4-deoxy-4-<(1R)-(1,5/4,6)-4,5,6-trihydroxy-3-hydroxymethyl-2-cyclohexenyl>amino-α-D-glucopyranoside 4',7':5',6'-di-O-isopropylidene derivative

(1S,2R,9S,10S)-9-amino-4,4,12,12-tetramethyl-3,5,11,13-tetraoxatricyclo[8.3.0.0^2,7]tridec-7-ene

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