3-methoxy-4-[(7-phenylheptyl)oxy]aniline

Base Information

• Chemical Name: 3-methoxy-4-[(7-phenylheptyl)oxy]aniline
• CAS No.: 15382-77-1
• Molecular Formula: C₂₀H₂₇NO₂
• Molecular Weight: 313.44
• Mol file: 15382-77-1.mol

Synonyms:m-Anisidine,4-[(7-phenylheptyl)oxy]- (6CI,8CI); 4-(7'-Phenylheptyloxy)-m-anisidine

Chemical Property of 3-methoxy-4-[(7-phenylheptyl)oxy]aniline

Chemical Property:

• Vapor Pressure: 2.56E-09mmHg at 25°C
• Boiling Point: 478.5°Cat760mmHg
• Flash Point: 269.6°C
• Density: 1.046g/cm³

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methoxy-4-[(7-phenylheptyl)oxy]aniline

There total 6 articles about 3-methoxy-4-[(7-phenylheptyl)oxy]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dichlorotetrahydro-2H-pyran (5631-95-8) → 1-Phenyl-7-<4-amino-2-methoxy-phenoxy>-heptan (15382-77-1)

Guidance literature:

Multi-step reaction with 5 steps

1: (i) Mg, Et₂O, (ii) Na

2: H₂ / Raney-Ni

3: aq. HBr, H₂SO₄

4: ethanol

5: H₂ / Raney-Ni

With sulfuric acid; hydrogen bromide; hydrogen; nickel; In ethanol;

DOI:10.1039/jr9610001863

Reference yield:

7-phenylheptan-1-ol (3208-25-1) → 1-Phenyl-7-<4-amino-2-methoxy-phenoxy>-heptan (15382-77-1)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. HBr, H₂SO₄

2: ethanol

3: H₂ / Raney-Ni

With sulfuric acid; hydrogen bromide; hydrogen; nickel; In ethanol;

DOI:10.1039/jr9610001863

Reference yield:

1-bromo-7-phenyl-heptane (78573-85-0) → 1-Phenyl-7-<4-amino-2-methoxy-phenoxy>-heptan (15382-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol

2: H₂ / Raney-Ni

With hydrogen; nickel; In ethanol;

DOI:10.1039/jr9610001863

upstream raw materials:

1-Phenyl-7-(4-nitro-2-methoxy-phenoxy)-heptan

2,3-dichlorotetrahydro-2H-pyran

7-phenylheptan-1-ol

1-bromo-7-phenyl-heptane