11-Azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane

Base Information

Chemical Name:11-Azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane
CAS No.:95617-30-4
Molecular Formula:C₁₀H₁₃N
Molecular Weight:147.22
Hs Code.:2912299000
DSSTox Substance ID:DTXSID70914908
ChEMBL ID:CHEMBL353418
Mol file:95617-30-4.mol

Synonyms:11-APCD;11-azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane;11-azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane hydrochloride;11-azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane picrate

Suppliers and Price of 11-Azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 11-Azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane

Chemical Property:

Vapor Pressure:0.0211mmHg at 25°C
Boiling Point:250.9°Cat760mmHg
Flash Point:103.6°C
PSA：12.03000
Density:1.277g/cm³
LogP:1.18740
XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:147.104799419
Heavy Atom Count:11
Complexity:236

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2C3CC4C1C5C2C3C4N5

Technology Process of 11-Azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane

There total 2 articles about 11-Azapentacyclo(6.2.1).0(2,7).0(4,10).0(5,9)decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 95617-28-0,95721-13-4
10-exo-hydroxytetracyclo<5.3.0.0.^2,60^4,9>decane 3-ketoxime

: 95617-30-4
11-azapentacyclo<6.2.1.0.^2,70.^4,100^5,9>decane

Guidance literature:: With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; for 7h; Heating;
DOI:10.1021/jm00383a022

Reference yield:

: 74069-58-2
10-exo-hydroxytetracyclo<5.3.0.0.^2,60^4,9>decan-3-one

: 95617-30-4
11-azapentacyclo<6.2.1.0.^2,70.^4,100^5,9>decane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NH₂OH*HCl, AcOK / methanol / Heating

2: 30 percent / LiAlH₄/H₂SO₄ / tetrahydrofuran / 7 h / Heating

With lithium aluminium tetrahydride; sulfuric acid; hydroxylamine hydrochloride; potassium acetate; In tetrahydrofuran; methanol;
DOI:10.1021/jm00383a022