1-(7-Hydroxy-9,10-dihydrophenanthren-2-yl)butan-1-one

Base Information

Chemical Name:1-(7-Hydroxy-9,10-dihydrophenanthren-2-yl)butan-1-one
CAS No.:7466-51-5
Molecular Formula:C₁₈H₁₈O₂
Molecular Weight:266.34
Hs Code.:
NSC Number:402643
DSSTox Substance ID:DTXSID60322992
Wikidata:Q82081791

Synonyms:7466-51-5;NSC 402643;NSC402643;1-(7-hydroxy-9,10-dihydrophenanthren-2-yl)butan-1-one;DTXSID60322992;NSC-402643

Suppliers and Price of 1-(7-Hydroxy-9,10-dihydrophenanthren-2-yl)butan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-(7-Hydroxy-9,10-dihydrophenanthren-2-yl)butan-1-one

Chemical Property:

Vapor Pressure:1.08E-09mmHg at 25°C
Boiling Point:476.2°Cat760mmHg
Flash Point:202.4°C
Density:1.162g/cm³
XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:266.130679813
Heavy Atom Count:20
Complexity:351

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(=O)C1=CC2=C(C=C1)C3=C(CC2)C=C(C=C3)O

Technology Process of 1-(7-Hydroxy-9,10-dihydrophenanthren-2-yl)butan-1-one

There total 2 articles about 1-(7-Hydroxy-9,10-dihydrophenanthren-2-yl)butan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5329-90-8
2-hydroxy-9,10-dihydrophenanthrene

: 141-75-3
butyryl chloride

: 7466-51-5
1-(7-hydroxy-9,10-dihydro-[2]phenanthryl)-butan-1-one

Guidance literature:: With aluminium trichloride; nitrobenzene; at 0 - 5 ℃; Erwaermen des Reaktionsprodukts mit methanol.KOH;
DOI:10.1080/01431160120769

Reference yield:

: 76302-58-4
9,10-dihydro-2-phenanthrenamine

: 7466-51-5
1-(7-hydroxy-9,10-dihydro-[2]phenanthryl)-butan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous HCl; NaNO₂ / Kochen der erhaltenen Diazoniumsalz-Loesung mit Wasser

2: AlCl₃; nitrobenzene / 0 - 5 °C / Erwaermen des Reaktionsprodukts mit methanol.KOH

With hydrogenchloride; aluminium trichloride; nitrobenzene; sodium nitrite;
DOI:10.1080/01431160120769