N-(2-Nitrophenyl)benzenecarbohydrazonoyl chloride

Base Information

Chemical Name:N-(2-Nitrophenyl)benzenecarbohydrazonoyl chloride
CAS No.:18468-66-1
Molecular Formula:C13H10ClN3O2
Molecular Weight:275.6904
Hs Code.:

Synonyms:BRN 0670013;N-(2-Nitrophenyl)benzenecarbohydrazonoyl chloride;Benzenecarbohydrazonoyl chloride, N-(2-nitrophenyl)-;18468-66-1;LS-29373

Suppliers and Price of N-(2-Nitrophenyl)benzenecarbohydrazonoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(2-Nitrophenyl)benzenecarbohydrazonoyl chloride

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:412.3°Cat760mmHg
Flash Point:203.2°C
Density:1.31g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:275.0461543
Heavy Atom Count:19
Complexity:337

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=NNC2=CC=CC=C2[N+](=O)[O-])Cl
Isomeric SMILES:C1=CC=C(C=C1)/C(=N/NC2=CC=CC=C2[N+](=O)[O-])/Cl

Technology Process of N-(2-Nitrophenyl)benzenecarbohydrazonoyl chloride

There total 1 articles about N-(2-Nitrophenyl)benzenecarbohydrazonoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18468-66-1
N¹-(2-nitrophenyl)-N²-α-chlorobenzylidenhydrazone

Guidance literature:: /BRN= 669405/, POCL3, 15-20grad, Py., 2h, 90-95grad;

Reference yield: 90.0%

: 18468-66-1
N¹-(2-nitrophenyl)-N²-α-chlorobenzylidenhydrazone

: 155951-41-0
N¹-(2-nitrophenyl)-N²-benzamidrazone

Guidance literature:: With ammonia; In 1,4-dioxane; for 1h; Ambient temperature;

Reference yield:

: 18468-66-1
N¹-(2-nitrophenyl)-N²-α-chlorobenzylidenhydrazone

: 2-phenyl-1,2,4-triazolo<1,5-a>quinoxaline

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / ammonia / dioxane / 1 h / Ambient temperature

2: 83 percent / diethyl ether; toluene / 4 h / Heating

3: 60 percent / iron, glacial acetic acid

4: 44 percent / LiAlH₄

5: 26 percent / glacial acetic acid / 0.08 h / Heating

With lithium aluminium tetrahydride; ammonia; iron; acetic acid; In 1,4-dioxane; diethyl ether; toluene;