Decahydro-4a,8a-butanonaphthalene

Base Information

Chemical Name:Decahydro-4a,8a-butanonaphthalene
CAS No.:13755-04-9
Molecular Formula:C14H24
Molecular Weight:0
Hs Code.:
Mol file:13755-04-9.mol

Synonyms:<4.4.4>Propellane;Tricyclo[4.4.4.0]tetradecan ([4.4.4]-Propellan);<4,4,4>Propellan;4.4.4-Propellan;Tricyclo<4.4.4.0>tetradecan (<4.4.4>-Propellan);Tricyclo[4.4.4.01,6]tetradecane;

Suppliers and Price of Decahydro-4a,8a-butanonaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Decahydro-4a,8a-butanonaphthalene

Chemical Property:

PSA：0.00000
LogP:4.68120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Decahydro-4a,8a-butanonaphthalene

There total 13 articles about Decahydro-4a,8a-butanonaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 88879-57-6
tricyclo<4.4.4.0>tetradecane-2,7-dione

: 13755-04-9
<4,4,4>propellane

Guidance literature:: With potassium hydroxide; hydrazine hydrate; In ethylene glycol; for 3h; Heating;

Reference yield:

: 15529-31-4
(1,4,5,8-tetrahydro-naphthalene-4a,8a-diyl)-bis-acetic acid anhydride

: 13755-04-9
<4,4,4>propellane

Guidance literature:: Multi-step reaction with 6 steps

1: Heating

2: (i) (COCl)2, benzene, (ii) /BRN= 102415/, THF, (iii) /BRN= 1098229/, Ag₂O

3: NaOMe / toluene / Heating

4: (i) aq. NaOH, EtOH, (ii) H₂SO₄

5: H₂ / Adams' catalyst / acetic acid

6: N₂H₄, KOH / ethane-1,2-diol / Heating

With potassium hydroxide; hydrogen; sodium methylate; hydrazine; platinum(IV) oxide; In ethylene glycol; acetic acid; toluene;
DOI:10.1016/0040-4020(68)88047-0

Reference yield:

: 15405-73-9
cis-1,6-bis(methoxycarbonylmethyl)bicyclo<4.4.0>deca-3,8-diene

: 13755-04-9
<4,4,4>propellane

Guidance literature:: Multi-step reaction with 6 steps

1: NaOMe / methanol; dioxane

2: (i) (COCl)2, benzene, (ii) /BRN= 102415/, THF, (iii) /BRN= 1098229/, Ag₂O

3: NaOMe / toluene / Heating

4: (i) aq. NaOH, EtOH, (ii) H₂SO₄

5: H₂ / Adams' catalyst / acetic acid

6: N₂H₄, KOH / ethane-1,2-diol / Heating

With potassium hydroxide; hydrogen; sodium methylate; hydrazine; platinum(IV) oxide; In 1,4-dioxane; methanol; ethylene glycol; acetic acid; toluene;
DOI:10.1016/0040-4020(68)88047-0