N-[(3S,4R,7R,8R,9S)-4,9-Dimethyl-2,6-dioxo-7-butyl-8-hydroxy-1,5-dioxonane-3-yl]-3-(formylamino)-2-hydroxybenzamide

Base Information

Chemical Name:N-[(3S,4R,7R,8R,9S)-4,9-Dimethyl-2,6-dioxo-7-butyl-8-hydroxy-1,5-dioxonane-3-yl]-3-(formylamino)-2-hydroxybenzamide
CAS No.:60504-95-2
Molecular Formula:C21H28N2O8
Molecular Weight:436.51
Hs Code.:
Mol file:60504-95-2.mol

Synonyms:Atrazine-desisopropyl;Atrazine-desisopropyl solution;deisovalerylblastmycin;deisovalerylblastomycin;deethyl simazine;2-Amino-4-chloro-6-ethylamino-s-triazine;desethyl simazine;Deisopropylatrazine;6-Deisopropylatrazine;6-chloro-N2-ethyl-1,3,5-triazine-2,4-diamine;

Suppliers and Price of N-[(3S,4R,7R,8R,9S)-4,9-Dimethyl-2,6-dioxo-7-butyl-8-hydroxy-1,5-dioxonane-3-yl]-3-(formylamino)-2-hydroxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DEISOVALERYLBLASTMYCIN 95.00%
5MG
$ 504.66

Total 5 raw suppliers

Chemical Property of N-[(3S,4R,7R,8R,9S)-4,9-Dimethyl-2,6-dioxo-7-butyl-8-hydroxy-1,5-dioxonane-3-yl]-3-(formylamino)-2-hydroxybenzamide

Chemical Property:

Vapor Pressure:1.89E-23mmHg at 25°C
Melting Point:187°C
Refractive Index:1.6500 (estimate)
Boiling Point:747.2°Cat760mmHg
PKA:7.28±0.50(Predicted)
Flash Point:405.7°C
PSA：158.24000
Density:1.32g/cm³
LogP:2.32750

Purity/Quality:

99% ^*data from raw suppliers

DEISOVALERYLBLASTMYCIN 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[(3S,4R,7R,8R,9S)-4,9-Dimethyl-2,6-dioxo-7-butyl-8-hydroxy-1,5-dioxonane-3-yl]-3-(formylamino)-2-hydroxybenzamide

There total 15 articles about N-[(3S,4R,7R,8R,9S)-4,9-Dimethyl-2,6-dioxo-7-butyl-8-hydroxy-1,5-dioxonane-3-yl]-3-(formylamino)-2-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₄N₂O₈

: 60504-95-2
deisovalerylblastomycin

Guidance literature:: With palladium on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 3h; under 760.051 Torr;
DOI:10.1002/ejoc.201100034

Reference yield:

: C₂₂H₄₃NO₅Si

: 60504-95-2
deisovalerylblastomycin

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

2: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

3: palladium on carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 760.05 Torr

With 4-methyl-morpholine; palladium on carbon; hydrogen; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100034

Reference yield:

: C₃₇H₅₄N₂O₈Si

: 60504-95-2
deisovalerylblastomycin

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

2: palladium on carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 760.05 Torr

With palladium on carbon; hydrogen; pyridine hydrogenfluoride; In tetrahydrofuran; ethyl acetate;
DOI:10.1002/ejoc.201100034