(E)-3-(5,6,7,8-tetrahydronaphthalen-2-yl)prop-2-enoic acid

Base Information

Chemical Name:(E)-3-(5,6,7,8-tetrahydronaphthalen-2-yl)prop-2-enoic acid
CAS No.:7498-69-3
Molecular Formula:C13H14O2
Molecular Weight:202.253
Hs Code.:
NSC Number:407569
DSSTox Substance ID:DTXSID50419709

Synonyms:NSC407569;7498-69-3;SCHEMBL7615401;DTXSID50419709;AKOS000346301;NSC-407569

Suppliers and Price of (E)-3-(5,6,7,8-tetrahydronaphthalen-2-yl)prop-2-enoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of (E)-3-(5,6,7,8-tetrahydronaphthalen-2-yl)prop-2-enoic acid

Chemical Property:

Vapor Pressure:1.67E-06mmHg at 25°C
Boiling Point:381.6°Cat760mmHg
Flash Point:280.5°C
Density:1.176g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:202.099379685
Heavy Atom Count:15
Complexity:257

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC2=C(C1)C=CC(=C2)C=CC(=O)O
Isomeric SMILES:C1CCC2=C(C1)C=CC(=C2)/C=C/C(=O)O

Technology Process of (E)-3-(5,6,7,8-tetrahydronaphthalen-2-yl)prop-2-enoic acid

There total 2 articles about (E)-3-(5,6,7,8-tetrahydronaphthalen-2-yl)prop-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

: 141-82-2
malonic acid

: 51529-97-6
5,6,7,8-tetrahydronaphthalene-2-carbaldehyde

: 7498-69-3
3-(6-Tetralyl)-2-propensaeure

Guidance literature:: With piperidine; In pyridine; at 80 ℃; for 24h;
DOI:10.1007/BF00810848

Reference yield:

: 141-82-2
malonic acid

: 51529-97-6
5,6,7,8-tetrahydronaphthalene-2-carbaldehyde

: 7498-69-3
3t-(5.6.7.8-tetrahydro-naphthyl-⁽²⁾)-acrylic acid

Guidance literature:: With piperidine; pyridine; Heating;
DOI:10.1021/jo00405a018

Reference yield:

: 7498-69-3
3-(6-Tetralyl)-2-propensaeure

: 2-(o-Carboxy-benzyliden)-(6,7,8,9-tetrahydrobenzo-indan)-1-on

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / Pd/C (10percent) / dioxane / 750.06 - 1500.1 Torr

2: polyphosphoric acid / 5 h / 80 °C

3: 63 percent / 1n NaOH / ethanol / 4 h / 0 °C

With sodium hydroxide; PPA; hydrogen; palladium on activated charcoal; In 1,4-dioxane; ethanol;
DOI:10.1007/BF00810848