1-Allyl-6-amino-3-methyl-5-nitroso-2,4(1H,3H)-pyrimidinedione

Base Information

Chemical Name:1-Allyl-6-amino-3-methyl-5-nitroso-2,4(1H,3H)-pyrimidinedione
CAS No.:90749-76-1
Molecular Formula:C₈H₁₀N₄O₃
Molecular Weight:210.192
Hs Code.:
NSC Number:95859
UNII:F29R438RQD
DSSTox Substance ID:DTXSID90238254
Wikidata:Q83120510

Synonyms:90749-76-1;1-Allyl-6-amino-3-methyl-5-nitroso-2,4(1H,3H)-pyrimidinedione;F29R438RQD;NSC95859;NSC 95859;UNII-F29R438RQD;NSC-95859;NCIOpen2_006216;DTXSID90238254;1-allyl-6-amino-3-methyl-5-nitroso-pyrimidine-2,4-dione;2,4(1H,3H)-PYRIMIDINEDIONE, 6-AMINO-3-METHYL-5-NITROSO-1-(2-PROPEN-1-YL)-;2,4(1H,3H)-PYRIMIDINEDIONE, 6-AMINO-3-METHYL-5-NITROSO-1-(2-PROPENYL)-;6-AMINO-3-METHYL-5-NITROSO-1-(2-PROPEN-1-YL)-2,4(1H,3H)-PYRIMIDINEDIONE

Suppliers and Price of 1-Allyl-6-amino-3-methyl-5-nitroso-2,4(1H,3H)-pyrimidinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of 1-Allyl-6-amino-3-methyl-5-nitroso-2,4(1H,3H)-pyrimidinedione

Chemical Property:

Vapor Pressure:0.00497mmHg at 25°C
Boiling Point:275.9°Cat760mmHg
Flash Point:120.6°C
Density:1.43g/cm³
XLogP3:-0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:210.07529019
Heavy Atom Count:15
Complexity:374

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=O)C(=C(N(C1=O)CC=C)N)N=O

Technology Process of 1-Allyl-6-amino-3-methyl-5-nitroso-2,4(1H,3H)-pyrimidinedione

There total 1 articles about 1-Allyl-6-amino-3-methyl-5-nitroso-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7052-53-1
1-allyl-3-methyl-6-amino uracil

: 90749-76-1
1-allyl-3-methyl-5-nitroso-6-amino uracil

Guidance literature:: With acetic acid; sodium nitrite; In water;
DOI:10.1021/jm00140a008

Reference yield:

: 90749-76-1
1-allyl-3-methyl-5-nitroso-6-amino uracil

: 90749-50-1
8-[3-(4-Benzhydryl-piperazin-1-yl)-propyl]-1,7-dimethyl-3-propyl-3,7-dihydro-purine-2,6-dione

Guidance literature:: Multi-step reaction with 7 steps

1: 96 percent / H₂ / Raney-NiW-2 / methanol / 4 h / 5320 Torr

2: 24 percent / 1.) 100 deg C, 4 h; 2.) 20 deg C, 20 h

3: 71 percent / 12N NaOH / H₂O / 2 h / 100 °C

4: 100 percent / K₂CO₃ / dimethylformamide / 3 h / 50 °C

5: 98 percent / H₂ / 5percent Pd/C / ethanol / 3 h / 20 °C / 6080 Torr

6: 70 percent / 48percent HBr, HBr (gas) / 20 h / Heating

7: 65 percent / methanol / 20 h / Heating

With sodium hydroxide; hydrogen bromide; hydrogen; potassium carbonate; palladium on activated charcoal; Raney-NiW-2; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(87)90056-0