Technology Process of 1-(Ethenesulfonyl)octadecane
There total 6 articles about 1-(Ethenesulfonyl)octadecane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonyl chloride; triethylamine;
In
dichloromethane;
at 20 ℃;
Cooling with ice;
DOI:10.1039/c0ob00355g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dihydrogen peroxide / acetic acid / 16 h / 20 °C / Darkness
2: methanesulfonyl chloride; triethylamine / dichloromethane / 20 °C / Cooling with ice
With
dihydrogen peroxide; methanesulfonyl chloride; triethylamine;
In
dichloromethane; acetic acid;
DOI:10.1039/c0ob00355g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / tetrahydrofuran; dimethyl sulfoxide / 16 h / 20 °C
2: dihydrogen peroxide / acetic acid / 16 h / 20 °C / Darkness
3: methanesulfonyl chloride; triethylamine / dichloromethane / 20 °C / Cooling with ice
With
dihydrogen peroxide; potassium carbonate; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; dichloromethane; acetic acid; dimethyl sulfoxide;
DOI:10.1039/c0ob00355g
