N,N-Diethyl-2-biphenylylamine

Base Information

• Chemical Name: N,N-Diethyl-2-biphenylylamine
• CAS No.: 6590-79-0
• Molecular Formula: C16H19N
• Molecular Weight: 225.334
• NSC Number: 6265
• DSSTox Substance ID: DTXSID40984375
• Nikkaji Number: J3.494.625F
• Wikidata: Q82971593

Synonyms:6590-79-0;N,N-Diethyl-2-biphenylylamine;NSC6265;SCHEMBL4817859;DTXSID40984375;NSC-6265;N,N-Diethyl[1,1'-biphenyl]-2-amine;J3.494.625F

Chemical Property of N,N-Diethyl-2-biphenylylamine

Chemical Property:

• Vapor Pressure: 5.53E-05mmHg at 25°C
• Boiling Point: 347°C at 760 mmHg
• Flash Point: 141.1°C
• Density: 0.998g/cm³
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 225.151749610
• Heavy Atom Count: 17
• Complexity: 204

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C1=CC=CC=C1C2=CC=CC=C2

Technology Process of N,N-Diethyl-2-biphenylylamine

There total 3 articles about N,N-Diethyl-2-biphenylylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

N,N-diethylaniline (91-66-7) → N,N-diethyl-[1,1'-biphenyl]-2-amine (6590-79-0) + 4-(N,N-diethylamino)biphenyl (5412-43-1) + N-ethyl-N-phenylamine (103-69-5) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

With Phenyl triflate; for 18h; Irradiation; further aryl perfluoroalkanesulfonate as reagent;

DOI:10.1016/0022-1139(93)02901-P

Reference yield: 21.0%

Phenyl triflate (17763-67-6) + N,N-diethylaniline (91-66-7) → N,N-diethyl-[1,1'-biphenyl]-2-amine (6590-79-0) + 4-(N,N-diethylamino)biphenyl (5412-43-1) + N-ethyl-N-phenylamine (103-69-5) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

for 18h; Irradiation;

DOI:10.1016/0022-1139(93)02901-P

Reference yield: 20.0%

Phenyl 1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoroethoxy) ethanesulfonate (105273-34-5) + N,N-diethylaniline (91-66-7) → N,N-diethyl-[1,1'-biphenyl]-2-amine (6590-79-0) + 4-(N,N-diethylamino)biphenyl (5412-43-1) + N-ethyl-N-phenylamine (103-69-5) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

for 20h; Irradiation;

DOI:10.1016/0022-1139(93)02901-P

upstream raw materials:

Phenyl triflate

N,N-diethylaniline

Phenyl 1,1,2,2-tetrafluoro-2-(1,1,2,2-tetrafluoroethoxy) ethanesulfonate

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