3,4-Dimethylphosphole manganese tricarbonyl

Base Information

Chemical Name:3,4-Dimethylphosphole manganese tricarbonyl
CAS No.:56993-57-8
Molecular Formula:C₉H₈MnO₃P
Molecular Weight:250.072
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Dimethylphosphole manganese tricarbonyl

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3,4-Dimethylphosphole manganese tricarbonyl

There total 1 articles about 3,4-Dimethylphosphole manganese tricarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 10170-69-1
dimanganese decacarbonyl

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 56993-57-8
3,4-dimethylphosphacymanthrene

: 110517-55-0
3,4-dimethyl-2-phenylphosphacymantrene

Guidance literature:: In toluene; High Pressure; heated at 150°C in a pressure vessel (CO pressure 3 atm); chromy. (hexane, second compd. = phenyl-substituted compd.), elem. anal.;
DOI:10.1016/0022-328X(86)80496-X

Reference yield: 85.0%

: 56993-57-8
3,4-dimethylphosphacymanthrene

: 2417-90-5
bromopropionitrile

: 591-51-5
phenyllithium

: 385832-60-0
(η4-1-phenyl-1-(2-cyanoethyl)-3,4-dimethylphospholium)tricarbonyl manganese

Guidance literature:: In tetrahydrofuran; to a soln. of complex in THF was added dropwise phenyllithium at -78°C, the mixt. was allowed to warm to room temp., treated with 3-bromopropionitrile, 30 min (inert atm.); the solvent was removed, extd. with CH2Cl2, washed with water, dried with MgSO4, chromd. on silica gel (CH2Cl2); elem. anal.;
DOI:10.1016/S0022-328X(01)01101-9