14-benzyloxymethoxy-10,12-O-carbonyl-4-N-imidazolylcarbonyl-6,7-isopropylidene-3,5,7,9,11,13-hexamethylhexadec-1-ene-4,6,7,10,12,14-hexol

Base Information

• Chemical Name: 14-benzyloxymethoxy-10,12-O-carbonyl-4-N-imidazolylcarbonyl-6,7-isopropylidene-3,5,7,9,11,13-hexamethylhexadec-1-ene-4,6,7,10,12,14-hexol
• CAS No.: 134916-12-4
• Molecular Formula: C₃₈H₅₆N₂O₉
• Molecular Weight: 684.871

Synonyms:14-benzyloxymethoxy-10,12-O-carbonyl-4-N-imidazolylcarbonyl-6,7-isopropylidene-3,5,7,9,11,13-hexamethylhexadec-1-ene-4,6,7,10,12,14-hexol

Chemical Property of 14-benzyloxymethoxy-10,12-O-carbonyl-4-N-imidazolylcarbonyl-6,7-isopropylidene-3,5,7,9,11,13-hexamethylhexadec-1-ene-4,6,7,10,12,14-hexol

Chemical Property:

• Vapor Pressure: 7.14E-21mmHg at 25°C
• Boiling Point: 725°Cat760mmHg
• Flash Point: 392.3°C
• PSA: 116.57000
• Density: 1.16g/cm³
• LogP: 7.77670

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 14-benzyloxymethoxy-10,12-O-carbonyl-4-N-imidazolylcarbonyl-6,7-isopropylidene-3,5,7,9,11,13-hexamethylhexadec-1-ene-4,6,7,10,12,14-hexol

There total 2 articles about 14-benzyloxymethoxy-10,12-O-carbonyl-4-N-imidazolylcarbonyl-6,7-isopropylidene-3,5,7,9,11,13-hexamethylhexadec-1-ene-4,6,7,10,12,14-hexol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,1'-carbonyldiimidazole (530-62-1) + (3S,4R,5S,6R,7R,9R,10S,11S,12R,13R,14R)-14-<(benzyloxy)methoxy>-6,7-(isopropylidenedioxy)-3,5,7,9,11,13-hexamethylhexadec-1-ene-4,10,12-triol → (3S,4R,5S,6R,7R,9R,10S,11S,12S,13S,14R)-14-<(benzyloxy)methoxy>-10,12-(carbonyldioxy)-3,5,7,9,11,13-hexamethyl-4-<((N-imidazolyl)carbonyl)oxy>-6,7-(isopropylidenedioxy)hexadecene (134916-12-4)

Guidance literature:

In benzene; for 20h; Heating;

DOI:10.1021/ja00090a016

Reference yield:

(3R,4R,5S,6R,8R,10R,11R,12S,13R,14S)-3-<(benzyloxy)methoxy>-5,13-dihydroxy-10,11-(isopropylidenedioxy)-4,6,8,10,12,14-hexamethylhexadec-15-en-7-one → (3S,4R,5S,6R,7R,9R,10S,11S,12S,13S,14R)-14-<(benzyloxy)methoxy>-10,12-(carbonyldioxy)-3,5,7,9,11,13-hexamethyl-4-<((N-imidazolyl)carbonyl)oxy>-6,7-(isopropylidenedioxy)hexadecene (134916-12-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Me₄NBH(OAc)3 / 1.) CH₃CN, AcOH, RT, 40 min, 2.) CH₃CN, AcOH, from -50 deg C to 10 deg C, 16 h

2: 98 percent / benzene / 20 h / Heating

With tetramethylammonium triacetoxyborohydride; In benzene;

DOI:10.1021/ja00090a016

upstream raw materials:

1,1'-carbonyldiimidazole

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