4H-Thieno(3,2-b)(1)benzazepine-4-propanamine, 9,10-dihydro-N,N-dimethy l-

Base Information

Chemical Name:4H-Thieno(3,2-b)(1)benzazepine-4-propanamine, 9,10-dihydro-N,N-dimethy l-
CAS No.:37968-12-0
Molecular Formula:C17H22N2S
Molecular Weight:286.435
Hs Code.:2934999090
Mol file:37968-12-0.mol

Synonyms:cyclohexane-1,4-diyldimethanediyl diprop-2-en-1-yl biscarbonate;Diallyl cyclohexane-1,4-diylbis(methylenecarbonate);[3-(9,10-dihydro-benzo[b]thieno[2,3-f]azepin-4-yl)-propyl]-dimethyl-amine;EINECS 253-089-5;

Suppliers and Price of 4H-Thieno(3,2-b)(1)benzazepine-4-propanamine, 9,10-dihydro-N,N-dimethy l-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 3 raw suppliers

Chemical Property of 4H-Thieno(3,2-b)(1)benzazepine-4-propanamine, 9,10-dihydro-N,N-dimethy l-

Chemical Property:

Vapor Pressure:7.65E-07mmHg at 25°C
Boiling Point:407.3°Cat760mmHg
Flash Point:200.1°C
PSA：71.06000
Density:1.107g/cm³
LogP:3.47120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
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Technology Process of 4H-Thieno(3,2-b)(1)benzazepine-4-propanamine, 9,10-dihydro-N,N-dimethy l-

There total 9 articles about 4H-Thieno(3,2-b)(1)benzazepine-4-propanamine, 9,10-dihydro-N,N-dimethy l- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 37968-01-7
9,10-dihydro-4H-thieno<3,2,b>benzazepine

: 109-54-6
3-(Dimethylamino)propyl chloride

: 37968-12-0
[3-(9,10-dihydro-benzo[b]thieno[2,3-f]azepin-4-yl)-propyl]-dimethyl-amine

Guidance literature:: With sodium hydride; In xylene; Heating;

Reference yield:

: 22751-23-1
(2-nitrophenyl)acetyl chloride

: 37968-12-0
[3-(9,10-dihydro-benzo[b]thieno[2,3-f]azepin-4-yl)-propyl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 8 steps

1: SnCl₄ / benzene / Ambient temperature

2: p-toluenesulfonic acid / 150 °C

3: 98 percent / Zn, CH₃COOH

4: DCC, / ethyl acetate

5: 1.) K₂CO₃, Cu, 2.) alkali / 1.) mesitylene, reflux, 22 h

6: 95 percent / HCl / ethanol

7: 100 percent / LiAlH₄, AlCl₃ / tetrahydrofuran / Ambient temperature

8: 100 percent / NaH / xylene / Heating

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; tin(IV) chloride; copper; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; acetic acid; dicyclohexyl-carbodiimide; zinc; In tetrahydrofuran; ethanol; ethyl acetate; xylene; benzene;

Reference yield:

: 38078-81-8
2-[2-(3-Bromo-thiophen-2-yl)-[1,3]dioxolan-2-ylmethyl]-phenylamine

: 37968-12-0
[3-(9,10-dihydro-benzo[b]thieno[2,3-f]azepin-4-yl)-propyl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 5 steps

1: DCC, / ethyl acetate

2: 1.) K₂CO₃, Cu, 2.) alkali / 1.) mesitylene, reflux, 22 h

3: 95 percent / HCl / ethanol

4: 100 percent / LiAlH₄, AlCl₃ / tetrahydrofuran / Ambient temperature

5: 100 percent / NaH / xylene / Heating

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; copper; sodium hydride; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; ethyl acetate; xylene;