13,14-Dihydro-2',14β-dihydroxy-4'',5''-dimethoxylythran-12-one

Base Information

• Chemical Name: 13,14-Dihydro-2',14β-dihydroxy-4'',5''-dimethoxylythran-12-one
• CAS No.: 15299-77-1
• Molecular Formula: C26H31 N O6
• Molecular Weight: 453.53
• Mol file: 15299-77-1.mol

Synonyms:Lythran-12-one,13,14-dihydro-2',14-dihydroxy-4'',5''-dimethoxy-, (14b)-; Lythridine (7CI,8CI); Sinine

Chemical Property of 13,14-Dihydro-2',14β-dihydroxy-4'',5''-dimethoxylythran-12-one

Chemical Property:

• Melting Point: 218-9°C

Purity/Quality:

99% ^*data from raw suppliers

Lythridine ≥98% ^*data from reagent suppliers

Safty Information:

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MSDS Files:

Useful:

• Description: Both Heirnia rnyritifolia Cham. et Schl. and H. salicifolia Link & Otto yield this macrocyc1ic alkaloid which may be crystallized from a mixture of AcOEt, MeOH and light petroleum as glistening needles. Two somewhat different values for the specific rotation have been recorded, viz. [α]25D - 174.2° (c 0.3325, CHC13) by Blomster and [α]25D - 153.4° (c 0.3, CHCI3) by Douglas. The ultraviolet spectrum exhibits a broad absorption maximum at 292 mil and an inflexion at 250 mil. Two methoxyl groups, a secondary and a phenolic hydroxyl group are present. The hydrochloride yields colourless crystals from MeOH, m.p. 330°C (dec.). The structure has been determined mainly from the infrared and mass spectra.

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