6-Aminophenanthridine

Base Information

• Chemical Name: 6-Aminophenanthridine
• CAS No.: 832-68-8
• Molecular Formula: C13H10 N2
• Molecular Weight: 194.236
• European Community (EC) Number: 809-749-5
• DSSTox Substance ID: DTXSID30232216
• Nikkaji Number: J50.001A
• Wikidata: Q83113249
• ChEMBL ID: CHEMBL3290780
• Mol file: 832-68-8.mol

Synonyms:6-aminophenanthridine;6AP phenanthridine cpd

Chemical Property of 6-Aminophenanthridine

Chemical Property:

• Vapor Pressure: 8.13E-07mmHg at 25°C
• Boiling Point: 406.4°C at 760 mmHg
• Flash Point: 228.6°C
• PSA: 39.64000
• Density: 1.268g/cm³
• LogP: 2.90030
• Storage Temp.: 2-8°C
• Solubility.: DMSO: soluble20mg/mL, clear
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 194.084398327
• Heavy Atom Count: 15
• Complexity: 229

Purity/Quality:

99% ^*data from raw suppliers

6-Aminophenanthridine ≥98% (HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T,Xi
• Hazard Codes: T,Xi
• Statements: 25-36
• Safety Statements: 26-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=CC=CC=C3N=C2N

Technology Process of 6-Aminophenanthridine

There total 22 articles about 6-Aminophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C21H18N2O → 6-aminophenanthridine (832-68-8)

Guidance literature:

With trifluoroacetic acid; at 20 ℃;

DOI:10.1016/j.bioorg.2021.105414

Reference yield: 56.0%

N-phenyl-2-(2-chlorophenyl)formamidine (23564-81-0) → 6-aminophenanthridine (832-68-8)

Guidance literature:

With ammonia; sodium amide; for 2h;

DOI:10.1016/j.tet.2004.03.062

Reference yield: 42.0%

2-Chlorobenzonitrile (873-32-5) + aniline (62-53-3) → 6-aminophenanthridine (832-68-8)

Guidance literature:

aniline; With ammonia; sodium amide; In diethyl ether; for 0.5h;

2-Chlorobenzonitrile; In diethyl ether; for 2h;

With lithium amide; In diethyl ether; for 2h; Further stages.;

DOI:10.1016/j.tet.2004.03.062

upstream raw materials:

phenanthridine

6-chlorophenanthridine

6-phenylphenanthridine

9-phenyl-9H-fluoren-9-amine

Downstream raw materials:

5-methyl-5H-phenanthridin-6-one-imine; hydriodide

di-phenanthridin-6-yl-amine

C₁₉H₁₃FN₄

C₁₉H₁₃BrN₄