o-Diacetotoluidide

Base Information

Chemical Name:o-Diacetotoluidide
CAS No.:3026-99-1
Molecular Formula:C11H13 N O2
Molecular Weight:191.23
Hs Code.:2925190090
DSSTox Substance ID:DTXSID80184352
Nikkaji Number:J837.752I
Wikidata:Q83055284
Mol file:3026-99-1.mol

Synonyms:o-Diacetotoluidide;3026-99-1;N-O-TOLYL-DIACETAMIDE;diacetyl-o-toluidine;SCHEMBL20657062;DTXSID80184352

Suppliers and Price of o-Diacetotoluidide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-ORTHO-TOLYL-DIACETAMIDE 95.00%
5MG
$ 497.65

Total 6 raw suppliers

Chemical Property of o-Diacetotoluidide

Chemical Property:

Boiling Point:105-105.5 °C(Press: 1.2 Torr)
PKA:0.29±0.50(Predicted)
PSA：37.38000
Density:1.118±0.06 g/cm3(Predicted)
LogP:1.89440
XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:191.094628657
Heavy Atom Count:14
Complexity:223

Purity/Quality:

99% ^*data from raw suppliers

N-ORTHO-TOLYL-DIACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1N(C(=O)C)C(=O)C

Technology Process of o-Diacetotoluidide

There total 10 articles about o-Diacetotoluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.88%

: 120-66-1
N-(2-methylphenyl)acetamide

: 108-24-7
acetic anhydride

: 3026-99-1
N-acetyl-N-(o-tolyl)acetamide

Guidance literature:: With pyridine; for 4h; Heating;

Reference yield: 48.0%

: (Z)-2,2,2-trifluoro-N-(o-tolyl)acetimidoyl chloride

: 3396-11-0
cesium acetate

: 51310-54-4
2-(trifluoromethyl)indole

: 3026-99-1
N-acetyl-N-(o-tolyl)acetamide

Guidance literature:: With bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis(2,6-diisopropylphenyl)dihydroimidazol-2-ylidene; In toluene; at 110 ℃; for 12h; Reagent/catalyst; Glovebox; Inert atmosphere;
DOI:10.1021/acs.orglett.6b00795