3-METHYL-6-NITRO-3H-BENZOTHIAZOL-2-YLIDENEAMINE

Base Information

• Chemical Name: 3-METHYL-6-NITRO-3H-BENZOTHIAZOL-2-YLIDENEAMINE
• CAS No.: 99700-95-5
• Molecular Formula: C₈H₇N₃O₂S
• Molecular Weight: 209.228
• Hs Code.: 2934999090
• Mol file: 99700-95-5.mol

Synonyms:3-methyl-6-nitro-3H-benzothiazol-2-one-imine;2-Imino-3-methyl-6-nitrobenzothiazoline;3-Methyl-6-nitro-3H-benzothiazol-2-on-imin;3-Methyl-6-nitro-3H-benzothiazol-2-ylideneamine;

Chemical Property of 3-METHYL-6-NITRO-3H-BENZOTHIAZOL-2-YLIDENEAMINE

Chemical Property:

• Vapor Pressure: 5.22E-05mmHg at 25°C
• Boiling Point: 347.9°Cat760mmHg
• Flash Point: 164.2°C
• PSA: 102.84000
• Density: 1.59g/cm³
• LogP: 2.25040

Purity/Quality:

99% ^*data from raw suppliers

3-METHYL-6-NITRO-3H-BENZOTHIAZOL-2-YLIDENEAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-METHYL-6-NITRO-3H-BENZOTHIAZOL-2-YLIDENEAMINE

There total 3 articles about 3-METHYL-6-NITRO-3H-BENZOTHIAZOL-2-YLIDENEAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-6-nitrobenzothiazole (6285-57-0) + dimethyl sulfate (77-78-1) → 3-methyl-6-nitro-3H-benzothiazol-2-one-imine (99700-95-5)

Guidance literature:

With benzene; at 60 ℃;

Reference yield:

2-Imino-3-methylbenzothiazolin (14779-16-9) → 3-methyl-6-nitro-3H-benzothiazol-2-one-imine (99700-95-5)

Guidance literature:

With nitric acid;

DOI:10.1039/jr9300002190

Reference yield:

ammonium thiocyanate (1147550-11-5) + N-methyl(p-nitroaniline) (100-15-2) → 3-methyl-6-nitro-3H-benzothiazol-2-one-imine (99700-95-5)

Guidance literature:

With ethanol; bromine; acetic acid;

upstream raw materials:

2-Imino-3-methylbenzothiazolin

2-amino-6-nitrobenzothiazole

dimethyl sulfate

ammonium thiocyanate

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