1,10-Phenanthroline-2-carboxylic acid

Base Information

Chemical Name:1,10-Phenanthroline-2-carboxylic acid
CAS No.:1891-17-4
Molecular Formula:C₁₃H₈N₂O₂
Molecular Weight:224.219
Hs Code.:2933990090
NSC Number:242683
UNII:N269GEQ2TJ
DSSTox Substance ID:DTXSID10172303
Nikkaji Number:J3.010.062J
Wikidata:Q83042414
Mol file:1891-17-4.mol

Synonyms:1,10-phenanthroline-2-carboxylic acid;2-carboxy-1,10-phenanthroline

Suppliers and Price of 1,10-Phenanthroline-2-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1,10-Phenanthroline-2-carboxylicacid 95+%
1g
$ 853.00

Arctom
1,10-Phenanthroline-2-carboxylicacid
1g
$ 807.00

American Custom Chemicals Corporation
1,10-PHENANTHROLINE-2-CARBOXYLIC ACID 95.00%
5MG
$ 500.69

Alichem
1,10-Phenanthroline-2-carboxylicacid
1g
$ 755.37

Total 27 raw suppliers

Chemical Property of 1,10-Phenanthroline-2-carboxylic acid

Chemical Property:

Vapor Pressure:1.57E-09mmHg at 25°C
Melting Point:209-210 °C
Boiling Point:467.2°Cat760mmHg
PKA:2.49±0.30(Predicted)
Flash Point:236.3°C
PSA：63.08000
Density:1.431g/cm³
LogP:2.48120
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:224.058577502
Heavy Atom Count:17
Complexity:308

Purity/Quality:

97% ^*data from raw suppliers

1,10-Phenanthroline-2-carboxylicacid 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C3=C(C=C2)C=CC(=N3)C(=O)O)N=C1

Technology Process of 1,10-Phenanthroline-2-carboxylic acid

There total 7 articles about 1,10-Phenanthroline-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1082-19-5
1,10-phenanthroline-2-carbonitrile

: 1891-17-4
1,10-phenanthroline-2-carboxylic acid

Guidance literature:: With hydrogenchloride; at 90 ℃; for 6h;
DOI:10.1002/adsc.200303134

Reference yield:

: 66-71-7
1,10-Phenanthroline

: 1891-17-4
1,10-phenanthroline-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen peroxide; acetic acid / water / 6 h / 70 °C

2: benzoyl chloride / water / 1 h / 20 °C

3: water; sodium hydroxide / ethanol / Reflux

With water; dihydrogen peroxide; benzoyl chloride; acetic acid; sodium hydroxide; In ethanol; water;
DOI:10.1039/c3dt50941a

Reference yield:

: 1891-19-6
1,10-phenanthroline N-oxide

: 1891-17-4
1,10-phenanthroline-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: benzoyl chloride / water / 1 h / 20 °C

2: water; sodium hydroxide / ethanol / Reflux

With water; benzoyl chloride; sodium hydroxide; In ethanol; water;
DOI:10.1039/c3dt50941a