o-ANISAMIDE, N-(CARBAMOYLMETHYL)-

Base Information

Chemical Name:o-ANISAMIDE, N-(CARBAMOYLMETHYL)-
CAS No.:6754-91-2
Molecular Formula:C10H12N2O3
Molecular Weight:208.2139
Hs Code.:
DSSTox Substance ID:DTXSID10217869
Wikidata:Q83094560

Synonyms:MOGN;N-(Carbamoylmethyl)-o-anisamide;o-ANISAMIDE, N-(CARBAMOYLMETHYL)-;2-methoxy-N-(methylcarbamoyl)benzamide;BRN 2582642;DTXSID10217869;LS-20046

Suppliers and Price of o-ANISAMIDE, N-(CARBAMOYLMETHYL)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of o-ANISAMIDE, N-(CARBAMOYLMETHYL)-

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.181g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:208.08479225
Heavy Atom Count:15
Complexity:243

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC(=O)NC(=O)C1=CC=CC=C1OC

Technology Process of o-ANISAMIDE, N-(CARBAMOYLMETHYL)-

There total 1 articles about o-ANISAMIDE, N-(CARBAMOYLMETHYL)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6754-91-2
2-o-Methoxybenzamidoacetamid

Guidance literature:: 2-Salicylamidoacetamid (XII), Dimethylsulfat, wss. NaOH, Δ;

Reference yield: 88.0%

: 60-29-7,927820-24-4
diethyl ether

: 6754-91-2
2-o-Methoxybenzamidoacetamid

: 97914-68-6
4-Ethoxy-2-(2-methoxy-phenyl)-1H-imidazole

Guidance literature:: With boron trifluoride diethyl etherate; epichlorohydrin; In dichloromethane; for 168h; Ambient temperature;
DOI:10.1248/cpb.36.1669

Reference yield:

: 6754-91-2
2-o-Methoxybenzamidoacetamid

: 97914-75-5
methyl (2-o-methoxyphenyl-6-ethoxycarbonyl-3,4-dihydro-4-oxopyrimidin-5-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₂O*BF₃, epichlorohydrin / CH₂Cl₂ / 168 h / Ambient temperature

2: 13 percent / toluene / 1 h / 50 - 60 °C

3: HCOOH / H₂O; dioxane / 2.5 h / 80 - 100 °C

With formic acid; boron trifluoride diethyl etherate; epichlorohydrin; In 1,4-dioxane; dichloromethane; water; toluene;
DOI:10.1248/cpb.36.1669