TR-2 Mycotoxin

Base Information

Chemical Name:TR-2 Mycotoxin
CAS No.:51177-07-2
Molecular Formula:C22H27N3O6
Molecular Weight:429.4663
Hs Code.:
NSC Number:353637
UNII:RTC582PPE3
DSSTox Substance ID:DTXSID901017899
Wikidata:Q105209759
Metabolomics Workbench ID:107200
Mol file:51177-07-2.mol

Synonyms:TR 2;TR-2 mycotoxin

Suppliers and Price of TR-2 Mycotoxin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of TR-2 Mycotoxin

Chemical Property:

Boiling Point:756.1°Cat760mmHg
Flash Point:411.1°C
PSA：126.33000
Density:1.52g/cm³
LogP:0.82320
XLogP3:-0.3
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:429.18998559
Heavy Atom Count:31
Complexity:776

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(CC1C2=C(C(C3(N1C(=O)C4CCCN4C3=O)O)O)C5=C(N2)C=C(C=C5)OC)O
Isomeric SMILES:CC(C)(C[C@H]1C2=C([C@@H]([C@@]3(N1C(=O)[C@@H]4CCCN4C3=O)O)O)C5=C(N2)C=C(C=C5)OC)O

Technology Process of TR-2 Mycotoxin

There total 3 articles about TR-2 Mycotoxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 117591-94-3
C₂₂H₂₅N₃O₄

: 115589-18-9,51177-07-2
Verruculogen TR-2

Guidance literature:: With osmium(VIII) oxide; In pyridine;
DOI:10.1016/S0040-4039(00)80288-9

Reference yield:

: 117611-42-4
8-(2'-hydroxy-2'-methylpropyl)-7,8,14,14a-tetrahydro-pyrrolidino-<1,2-c>-piperazino-<1',6'-2,3>-β-carboline-(5aHα, 8Hα, 14aHβ)-1,6-dione

: 115589-18-9,51177-07-2
Verruculogen TR-2

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / 2,3,4,5,6,6-hexachloro-2,4-cyclohexadien-1-one / CH₂Cl₂ / 0.5 h

2: 46 percent / trifluoroacetic acid / CH₂Cl₂ / 1 h / Ambient temperature

3: 1) osmium tetroxide, 2) aq. NaHSO₃ / 1) pyridine, 0 deg C, 2 h, 2) room temperature, 30 min

With osmium(VIII) oxide; 2,2,3,4,5,6-hexachloro-cyclohexa-2,4-dien-1-one; sodium hydrogensulfite; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo00040a030

Reference yield:

: 117591-95-4
C₂₃H₂₉N₃O₅

: 115589-18-9,51177-07-2
Verruculogen TR-2

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / trifluoroacetic acid / CH₂Cl₂ / 1 h / Ambient temperature

2: 1) osmium tetroxide, 2) aq. NaHSO₃ / 1) pyridine, 0 deg C, 2 h, 2) room temperature, 30 min

With osmium(VIII) oxide; sodium hydrogensulfite; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo00040a030