(1S,3S)-3-ACETYL-2,2-DIMETHYLCYCLOBUTANE ACETONITRILE

Base Information

• Chemical Name: (1S,3S)-3-ACETYL-2,2-DIMETHYLCYCLOBUTANE ACETONITRILE
• CAS No.: 39863-94-0
• Molecular Formula: C10H15NO
• Molecular Weight: 165.23
• Hs Code.: 29269095
• Mol file: 39863-94-0.mol

Synonyms:cis-1-Acetyl-3-cyanomethyl-2,2-dimethylcyclobutan;cis-1-Acetoxy-1-hepten;1c-Acetoxy-hept-1-en;

Chemical Property of (1S,3S)-3-ACETYL-2,2-DIMETHYLCYCLOBUTANE ACETONITRILE

Chemical Property:

• Vapor Pressure: 0.00617mmHg at 25°C
• Refractive Index: 1.463-1.465
• Boiling Point: 272.2°C at 760 mmHg
• Flash Point: 118.4°C
• PSA: 40.86000
• Density: 0.962g/cm³
• LogP: 2.54148
• Storage Temp.: Refrigerator (+4°C)

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-((1S,3S)-3-Acetyl-2,2-dimethylcyclobutyl)acetonitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn,T
• Statements: 20/21/22-25
• Safety Statements: 24/25-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1S,3S)-3-ACETYL-2,2-DIMETHYLCYCLOBUTANE ACETONITRILE

There total 4 articles about (1S,3S)-3-ACETYL-2,2-DIMETHYLCYCLOBUTANE ACETONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-morpholinopinan-3-one oxime (131488-84-1) → (1S,3S)-3-acetyl-2,2-dimethylcyclobutaneacetonitrile (39863-94-0,368423-20-5) + (1S,3S)-3-acetyl-2,2-dimethylcyclobutaneacetonitrile (4426-04-4,28353-00-6,39863-94-0,131488-86-3,138512-75-1,368423-20-5)

Guidance literature:

With phosphorus pentachloride; In chloroform; at -25 ℃; for 1.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

2-morpholinopinan-3-one oxime (131488-84-1) → (1S,3S)-3-acetyl-2,2-dimethylcyclobutaneacetonitrile (39863-94-0,368423-20-5) + (1S,3S)-3-acetyl-2,2-dimethylcyclobutaneacetonitrile (4426-04-4,28353-00-6,39863-94-0,131488-86-3,138512-75-1,368423-20-5)

Guidance literature:

With phosphorus pentachloride; In chloroform; at -25 ℃; for 1.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

(+)-α-pinene (7785-70-8,25766-18-1) + lead(IV) tetraacetate (546-67-8) → (1S,3S)-3-acetyl-2,2-dimethylcyclobutaneacetonitrile (39863-94-0,368423-20-5)

Guidance literature:

With trimethylsilylazide; In acetonitrile;

upstream raw materials:

(+)-α-pinene

lead(IV) tetraacetate

2-morpholinopinan-3-one oxime

Refernces