1,4-Diacetylbenzene dioxime

Base Information

• Chemical Name: 1,4-Diacetylbenzene dioxime
• CAS No.: 27912-60-3
• Molecular Formula: C10H12 N2 O2
• Molecular Weight: 192.217
• Hs Code.: 2928000090
• Mol file: 27912-60-3.mol

Synonyms:Benzene,p-diacetyl-, dioxime (6CI,8CI); Ethanone, 1,1'-(1,4-phenylene)bis-, dioxime(9CI); 1,4-Diacetylbenzene dioxime; NSC 133092; p-Diacetylbenzene dioxime

Chemical Property of 1,4-Diacetylbenzene dioxime

Chemical Property:

• Vapor Pressure: 4.86E-05mmHg at 25°C
• Melting Point: 248-250 °C
• Boiling Point: 311.8°Cat760mmHg
• PKA: 10.97±0.70(Predicted)
• Flash Point: 142.4°C
• PSA: 65.18000
• Density: 1.14g/cm³
• LogP: 2.08300

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4-Diacetylbenzene dioxime

There total 2 articles about 1,4-Diacetylbenzene dioxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,4-Diacetylbenzene (1009-61-6) → 1,4-diacetylbenzene dioxime (27912-60-3)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; In methanol; at 20 ℃; Green chemistry;

DOI:10.1039/c3ra40585k

Reference yield:

→ 1,4-diacetylbenzene dioxime (27912-60-3)

Guidance literature:

p-Diacetylbenzol, Hydroxylamin-Sulfat, wss. Ethanol, 2,5-stdg. kochen;

Reference yield: 95.0%

lithium tetrachloropalladate + 1,4-diacetylbenzene dioxime (27912-60-3) → catena-μ-(1,4-diacetylbenzenedioxime-C(4),N:C(6),N')di-μ-chloro-dipalladium(II)

Guidance literature:

In methanol; elem. anal.;

DOI:10.1016/0022-328X(91)80010-H

upstream raw materials:

1,4-Diacetylbenzene

Downstream raw materials:

2H,2'H-3,3'-p-phenylene-bis-isoxazol-5-one

1,4-bis(1-vinyl-1H-pyrrol-2-yl)benzene

N,N'-diacetyl-1,4-phenylenediamine

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