24-Nor-6,7-secochola-14,20,22-triene-3,6-diol, 7-(((2-chlorophenyl)methyl)amino)-21,23-epoxy-4,4,8-trimethyl-, (3-beta,5-beta,13-alpha,17-alpha)-

Base Information

Chemical Name:24-Nor-6,7-secochola-14,20,22-triene-3,6-diol, 7-(((2-chlorophenyl)methyl)amino)-21,23-epoxy-4,4,8-trimethyl-, (3-beta,5-beta,13-alpha,17-alpha)-
CAS No.:90294-21-6
Molecular Formula:C₃₃H₄₆ClNO₃
Molecular Weight:540.186
Hs Code.:

24-Nor-6,7-secochola-14,20,22-triene-3,6-diol, 7-(((2-chlorophenyl)methyl)amino)-21,23-epoxy-4,4,8-trimethyl-, (3-beta,5-beta,13-alpha,17-alpha)-

Synonyms:

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Chemical Property of 24-Nor-6,7-secochola-14,20,22-triene-3,6-diol, 7-(((2-chlorophenyl)methyl)amino)-21,23-epoxy-4,4,8-trimethyl-, (3-beta,5-beta,13-alpha,17-alpha)-

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MSDS Files:: SDS file from LookChem

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Technology Process of 24-Nor-6,7-secochola-14,20,22-triene-3,6-diol, 7-(((2-chlorophenyl)methyl)amino)-21,23-epoxy-4,4,8-trimethyl-, (3-beta,5-beta,13-alpha,17-alpha)-

There total 3 articles about 24-Nor-6,7-secochola-14,20,22-triene-3,6-diol, 7-(((2-chlorophenyl)methyl)amino)-21,23-epoxy-4,4,8-trimethyl-, (3-beta,5-beta,13-alpha,17-alpha)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 90294-14-7
(R)-6-((1R,4R,7aS)-4-{[(E)-2-Chloro-benzylimino]-methyl}-1-furan-3-yl-4,7a-dimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-5-yl)-2,2,6-trimethyl-3-oxo-cyclohexanecarbaldehyde

: 90294-21-6
(R)-4-{(1R,4R,7aS)-4-[(2-Chloro-benzylamino)-methyl]-1-furan-3-yl-4,7a-dimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-5-yl}-3-hydroxymethyl-2,2,4-trimethyl-cyclohexanol

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 1h; Heating;

Reference yield:

: 62655-07-6,90365-38-1
dysobindialdehyde

: 90294-21-6
(R)-4-{(1R,4R,7aS)-4-[(2-Chloro-benzylamino)-methyl]-1-furan-3-yl-4,7a-dimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-5-yl}-3-hydroxymethyl-2,2,4-trimethyl-cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / ethanol / 3 h / 60 - 70 °C

2: 70 percent / sodium borohydride / ethanol / 1 h / Heating

With sodium tetrahydroborate; In ethanol;

Reference yield:

: 89-97-4
2-CHLOROBENZYLAMINE

: 90294-21-6
(R)-4-{(1R,4R,7aS)-4-[(2-Chloro-benzylamino)-methyl]-1-furan-3-yl-4,7a-dimethyl-2,4,5,6,7,7a-hexahydro-1H-inden-5-yl}-3-hydroxymethyl-2,2,4-trimethyl-cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / ethanol / 3 h / 60 - 70 °C

2: 70 percent / sodium borohydride / ethanol / 1 h / Heating

With sodium tetrahydroborate; In ethanol;