[(E)-cyclohexylmethylideneamino]urea

Base Information

• Chemical Name: [(E)-cyclohexylmethylideneamino]urea
• CAS No.: 3183-63-9
• Molecular Formula: C8H15N3O
• Molecular Weight: 169.227
• NSC Number: 408596
• DSSTox Substance ID: DTXSID10430450
• Mol file: 3183-63-9.mol

Synonyms:NSC408596;3183-63-9;SCHEMBL20598139;DTXSID10430450;AKOS008939737;NSC-408596

Chemical Property of [(E)-cyclohexylmethylideneamino]urea

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.24g/cm³
• XLogP3: 1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 169.121512110
• Heavy Atom Count: 12
• Complexity: 173

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)C=NNC(=O)N
• Isomeric SMILES: C1CCC(CC1)/C=N/NC(=O)N

Technology Process of [(E)-cyclohexylmethylideneamino]urea

There total 10 articles about [(E)-cyclohexylmethylideneamino]urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-oxaspiro(2.5)octane (185-70-6) → cyclohexanecarbaldehyde-semicarbazone (3183-63-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ZnCl₂

With zinc(II) chloride;

DOI:10.1021/ja01371a070

Reference yield:

cyclohexanecarbaldehyde (2043-61-0) → cyclohexanecarbaldehyde-semicarbazone (3183-63-9)

Guidance literature:

DOI:10.1021/ja01371a070 DOI:10.1021/ja01169a522

Reference yield:

→ cyclohexanecarbaldehyde-semicarbazone (3183-63-9)

Guidance literature:

With ethanol; palladium; Hydrogenation;

upstream raw materials:

cyclohexanecarbaldehyde

1-oxaspiro(2.5)octane

ethyl (2-chlorocyclohexylidene)acetate

2-cyclohexyl-2-oxoethanoic acid

Downstream raw materials:

cyclohexanecarbaldehyde

methyl (2-(2-(cyclohexylmethylene)hydrazono)-4-oxothiazolidin-5-ylidene)acetate

Refernces